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GC/MS analysis results for sample AD23499, Oct 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23499 conducted on October 19, 2001.

NYC-WTC_000088799–000088825

Folder label: “GC/MS Scan 9/27/01

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Scanned page image, NYC-WTC_000088816
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NYC 9/11 Public Portal Document

-Library—Search-Gompound Report Data File : C:\HPCHEM\1\DATA\OCT1601\23499.D Vial: 7 Acq On : 16 Oct 2001 8:06 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P

Quant Method ; C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 11 Heneicosane Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 32.73 4.41 ug/1 534181 Chrysene-dl2 33.12 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Heneicosane 296 C21H44 000629-94-7 91\ 2 Octadecane 254 C18H38 000593-45-3 9R 3 Tetracosane 338 C24H50 000646-31-1 90 4 Hexatriacontane_____________________ 507 C36H74 000630-06-8 87 <\bundance Scan 3016 (32.729 min): 23499.D (-) m/z 57.00 100.00% 7

5000 85

4' -r-r-p-r-n-f- R T 32.40 32.60 32.80 33.00 RRRJ^XXSI225 252267 ^5_ 11T11,... f 11111, r, 1111.. I,,,. I., I, I,,,. I,,,. I,,., I,,,, I,, 352 m/z 71.00 69733% '''' I n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 ^bundance #42201: Heneicosane 57

5000 85 RX 32.40 32.60 32.80 33.00 m77 43.00 63.75% 268 296 * I ' •TI I I I I • fI I I I I I" " I" " I" " I I " '' I " ' ' I' n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance — — #71561: Octadecane 517 \\

32.40 32,60 32,80 33.00 85 5000 Wz 85705 48.84%

224 254 n/z-> 40 60 4 ' I ''' ‘ I'''' I 80 100 120 140 160 180 200 220 240 260 280 300 320 340 p-rTTj-n-n-p

Abundance 7- #73543:Tetracosane——------- -- RX I ' ' ' 'T I 'J ' I ~ 32.40 32.60 32.80 33.00^ 7n7z 41.05 25.41%

553 _85„

I I 113 294155 183 338 I' I'’ T" I' " '.I' pn-TTj- ■nZz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 32.40 32.60 32.80 33.00

23499.D NP091101.M Thu Oct 18 10:14:26 2001 Page 11

NYC-WTC_000088816

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NYC-WTC_000088816Source: NYC Law Department, mirrored locally

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