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GC/MS analysis results for sample AD23498, Oct 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23498 conducted on October 19, 2001.

NYC-WTC_000088774–000088798

Folder label: “GC/MS Scan 9/27/01

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Scanned page image, NYC-WTC_000088793
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File ; C;\HPCHEM\1\DATA\OCT1601\23498 .D Vial: 6 Acq On : 16 Oct 2001 7:07 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 13 Heneicosane Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 34.61 2.57 ug/1 294999 Chrysene-dl2 33.12 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Heneicosane 296 C21H44 000629-94-7 9f 2 Heptadecane 240 C17H36 000629-78-7 91 3 Pentacosane 352 C25H52 000629-99-2 91 4 Tetracosane ____________________ 338 C24H50 _______ 00064623121 90 Abundance Scan 3221 (34.608 min); 23498. D (-) m/z SYTOO 100.00% 7 43 71

5000 85

, .1 Ji. T 'T/'..rH\''.?^169183 197 211 225 34.20 34.40 34.60 34.80 35.00 256 281 m/z ' ' 'P ' ' Tp-rVrYTV-rfY-r-r^H-yT*VT-T-fT-TTVp-T*Tnry-rTT-rTT--rT^^ ' ' I ' ' ' ' I ' ' 71.00 71.44% Ti/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #42201: Heneicosane 57 71 85 553 34.20 34.40 34.60 34,80 35.00 99 m/z 43.05 69.60% I il J I''' ‘ I'''' I''' ' I 268 pr-nr-r-p-T-rt-p- 296 ■n^-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 /Abundance #71193:Heptadec^ 7 I 71 34.20 34.40 3460 34.80 35.00 5000 ■m/z 85.05 49.56% 85

99 I J ■'27 141 155169 210 240 r '' ' I'' I' I'' 111'...I., I pnrn-rp-rrn-l-r- I ' ' ' ' I tVz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #73718; Pentacosane 43 5,7 34.20 34.40 34.60“34.80~^35.00" ■m/z 41.05 26.89% 71 5000 85

TT-p-r , j, , t 225........... Tl/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 34.20 34.40 34.60 34.80 35.00

23498.D NP091101.M Thu Oct 18 10:10:55 2001 Page 13

NYC-WTC_000088793

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NYC-WTC_000088793Source: NYC Law Department, mirrored locally

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