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GC/MS analysis results for sample AD23650, Oct 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23650 conducted on October 19, 2001.

NYC-WTC_000089000–000089024

Folder label: “GC/MS Scan 9/27/01

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Scanned page image, NYC-WTC_000089021
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NYC 9/11 Public Portal Document

Library Search Compound_Repor.t. Data File : C:\HPCHEM\1\DATA\OCT1601\23650.D Vial: 15 Acq On : 17 Oct 2001 3:56 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 15 Pentatriacontane Concentration Rank 11 R.T. EstConc Area Relative to ISTD R.T. 36.37 0.57 ug/1 60399 Perylene-dl2 37.24

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

/ y Pentatriacontane 493 C35H72 000630-07-9 91 ^2 Triacontane 422 C30H62 000638-68-6 90 3 Nonacosane 408 C29H60 000630-03-5 90 4 Tritetracontane 605 C43H88 007098-21-7 90 Abundance Scan 3412 (36.367 min): 23650.D (-) m/z 57795 177/00%

85

'1' 36.00 36.20 36.40 36.60 208 p-n-r m/z 71.10 79.28% nZz-> 40 60 80 100120140160180200 220240260 280300320 340360380 400420 Abundance #58743: Pentatriacontane 7

5000 ■ , , 01 , , 85 36W36J0 36.40 36.60 m/ Z 43.00 61.43% i II I 1^1 . 169 197 225______________________

n/z-> 40 60 80 100120140160180200 220240 260 280300320 340360380 400420 Abundance- --- ---- -—-- - -- #55461: Triacontane - - -- - 4b

71 36.00 36.20 36.40 36.60 5000 m/z 85.05 54.48%

Ti/z-> "' I' " LUX 239 267 I" " I" " I' 11,111" 11" 11111111 "■ 11 ■ 40 60 80 100120140160180200 220240260 280300320 340360380 400420 379 I (11" 111111" III" " I ■ "' I" " I ‘ 422 ‘I"‘ I I I I /i P....................... ... Abundance _ ___ ._#54526: Nonacosane__ 43 -36 00. 36.20 - 36.40 36 60 m/z 55.00 25767% 71 5000

I 1 127 211 239 379 408 A...... N '"I"' " I" " I" " I"' I" " I"'' I “ " i" " I" " I" " I" " I" " r "' I" " I"' n^-> 40 60 80 100120140160180 200 220240260280300320 340360380 400420 36.00 36.20 36.40 36.60

23650.D NP091101.M Thu Oct 18 10:40:35 2001 Page 15

NYC-WTC_000089021

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NYC-WTC_000089021Source: NYC Law Department, mirrored locally

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