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GCMS analysis comments for sample AD28688, Dec 2001

Machine-extracted title · confidence 100%

Laboratory report noting di-n-butylphthalate detection and TurboVap contamination with recovery data for sample AD28688.

NYC-WTC_000035026–000035043

Folder label: “GCMS X 11/24/01 A 12/4/01

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Scanned page image, NYC-WTC_000035036
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC0401\28688.D Vial: 6 Acq On 4 Dec 2001 5:15 pm Operator: 209 GALOS Sample : gc/ms 11/24 Inst : GC/MS 209 Misc Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 Tricosane Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T. --------------------------------------------------------------------- 30.63 0.68 ug/l 136093 Chrysene-d12 33.04

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Tricosane 324 C23H48 000638-67-5 06 2 Pentacosane 352 C25H52 000629-99-2 91 3 Hexatriacontane 507 C36H74 000630-06-8 91 4 Docosane, 11-but l- 366 C26H54 013475-76-8 91 bundance Scan 2787 (30.634 min): 28688.D (-) m z 56. 95 100.00% rf 43 71 85 5000

, J 40 60 80 99 113127141 155169183197 224 100 120 140 160 180 200 220 240 260 280 300 320 324 m/z 30.40 30.60 30.80 31.00 43.00 76.05% 0

undance #73318:Tricosane

71 5000 85 30.40 30.60 30.80 31.00 m/z 71.00 70.00% 99113127141 183197211225 296 324 Liz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 ¼bundance #73718: Pentacosane

71 30.40 30.60 30.80 31.00 5000 85 m/z 85.00 56.68%

99 113127141155169183197211225 rift-> 40_60 80 100 120 140 160 180 200 220 240 260 280 300 320 undance #74636: Hexatriacontane 30.40 30.60 30.80 31.00 m/z 41.05 33.51% 71 5000 85

99 113127 141155169183197211 I I I I I I I I I I I I I I I I I I I I p I I I

-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 30.40 30.60 30.80 31.00

28688.D . GCMS1126.M Thu Dec 06 .13:23:14 2001 Page 5

NYC-WTC 000035036

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NYC-WTC_000035036Source: NYC Law Department, mirrored locally

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