GC/MS chromatogram data for lab blank 9/25, Oct 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1201\LB.D vial: 12 Acq On : 12 Oct 2001 12:53 pm Operator: 209 GALOS Sample : lab blk 9/25 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C;\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 Tricosane Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T. 30.70 1.67 ug/1 304132 Chrysene-dl2 33.13 Hit# of 5 Tentative ID MW MolForm CAS# Qual ( 1 yiricosane 324 C23H48 000638-67-5 95 2- Eicosane 282 C20H42 000112-95-8 91 3 Octadecane 254 C18H38 000593-45-3 91 4 Heptadecane 240 C17H36 _____ 000629-78-7 91 Abundance Scan 2795 (30.703 min): LB.D (-) m/z 57700 100.00% 57 71 A 43 5000 85

’"m' I 99 30.40 30.60 30.80 31.00 ■II I. i M. A■ 324 I I I I T I I T” I |Ti I I I I I T I I I I > I I I I I I I I r I I I I I I I I I I I I I I I > I I I I I I I I I I I I I I I I I 1 1 -rq-n-i m/z71.10 70.80% Tife-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #73318: Tricosane 43 57

71 5000 85 30.40 30.60 30.80 31.00 m/z 43705 66.55% 99 I III J'If'’ 1^197211^ 296 324 TVry‘^rTVYrTT4-p-H-TqHnT-rj-TTn-TyVrTT‘jTTY-rp*T-TTq-rTTT-YTTT-TYrTn^^ ■nfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #39862: Eicosane 43 57

71 77 P ' ' T 30.40 30.60 30.80 31.00 5000 85 m/z 85.05 49.64%

1 113127141155 196 I'''' I' 240 r-rp- 282 ' I ' ' ' ' I ' ' ' ' I ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #71561: Octadecane 57 30.40 30.60 30.80 31.00 43 71 m/z41.05 26.53% I 85 5000

99 224 254 ' I ' ' ' ' I ' ' ' ' I ' • ' ' ! ' I''' ‘ r ''' I'''' I' ‘' I'''' I ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 30.40 30.60 30.80 31.00

LB.D NP091101.M Mon Oct 15 15:00:50 2001 Page 7

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