NYC-WTC_000009667
Calibration table page listing internal standards and response factors for GCMS analysis.
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GCMS calibration table for TCLP analysis, Feb 2002
Machine-extracted title · confidence 100%Calibration data table for GC/MS analysis of TCLP samples listing retention times and response values for deuterated standards.
NYC-WTC_000038116–000038118Folder label: “GCMS X 2/21/02 A 2/22/02”
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NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File : C:\HPCHEM\l\DATA\FEB2102\REFB2.D Vial: 32 Acq On : 22 Feb 2002 9:42 pm Operator: Sample : gc/ms scan 2/21 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 27 11:15 2002 Quant Results File: GCMS0208.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Thu Feb 21 16:13:52 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208
Compound R.T. Qlon Response Cone Unit Qvalue
30) N-Nitrosodiphenylamine 23.31 168 108187 5.66 ug/1 # 88 31) 4-Bromophenyl-phenylether 24.39 248 65541 5.30 ug/1 97 3 2) Hexachlorobenzene 24.82 284 75871 5.24 ug/1 99 3 3) Phenanthrene 25.81 178 374272 6.34 ug/1 99 34) Anthracene 25.93 178 365003 6.32 ug/1 99 35) Di-n-butylphthalate 27.70 149 516048 6.26 ug/1 99 36) Fluoranthene 29.43 202 363610 6.17 ug/1 # 91 3 9) Pyrene 30.11 202 379783 6.73 ug/1 # 89 40) Butylbenzylphthalate 32.23 149 185438 5.93 ug/1 95 41) Benzo(a)anthracene 33.75 228 256594 6.22 ug/1 99 42) Bis(2-ethylhexyl)phthalate 34.00 149 216633 5.13 ug/1 97 43) Chrysene 33.88 228 272172 6.70 ug/1 100 45) Di-n-Octylphthalate 35.75 149 257552 3.81 ug/1 98 4 6) Benzo(b)fluoranthene 36.87 252 204347 5.36 ug/1 # 96 47) Benzo(k)fluoranthene 36.94 252 247591 6.46 ug/1 # 96 48) Benzo(a)pyrene 37.88 252 166508 5.27 ug/1 # 95 49) Indeno(1,2,3-cd)pyrene 42.28 276 158455 5.50 ug/1 # 93 5 0) Dibenz(a,h)anthracene 42.36 278 129401 5.87 ug/1 # 93 51) Benzo(g,h,i)perylene 43.54 276 137137 5.90 ug/1 # 93
(#) = qualifier out of range (m) = manual integration REFB2.D GCMS0208.M Wed Feb 27 11:18:28 2002 Page 2
NYC-WTC_000038117
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