GCMS calibration results for sample AE03078, March 2002

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Laboratory report showing GC/MS calibration data and surrogate recovery for sample AE03078 on March 22, 2002.

NYC-WTC_000011132–000011134

Folder label: “GCMS X 2/12/02 A 3/19/02”

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Quantitation Report (QT Reviewed) J . $ Data File C:\HPCHEM\l\DATA\MAR0102\3078 .D Vial: 30 Acq On 2 Mar 2002 2:50 pm Operator : Sample gc/ms scan 2/12 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 5 14:14 2002 Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Feb 27 11:30:15 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.31 152 446870 20.00 ug/1 -0.04 10) Naphthalene-d8 15.96 136 1758319 20.00 ug/1 -0.04 17) Acenaphthene-diO 21.27 164 934811 20.00 ug/1 -0.04 29) Phenanthrene-diO 25.72 188 1359150 20.00 ug/1 -0.05 38) Chrysene-dl2 33.79 240 927975 20.00 ug/1 -0.06 44) Perylene-dl2 38.06 264 617967 20.00 ug/1 -0.07

System Monitoring Compounds 37) 2,4-DDD 30.79 235 65438 4.61 ug/mL 0.30 Spiked Amount 5.000 Recovery = 92.20%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybi s(1-Chioropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) 1sophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 0.00 128 0 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 20.63 163 1639 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 2 2) Acenaphthylene 0.00 152 0 N.D. 2 3) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.74 149 3966 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.

(#) = qualifier out of range (m) = manual integration 3078.D GCMS0208.M Tue Mar 05 14:15:37 2002 Page 1

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