GCMS VOC Analysis Results, March 8 2002

NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\FEB2102\REFC2.D Vial: 46 Acq On : 23 Feb 2002 1:26 pm Operator: Sample : gc/ms scan 1/14 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 8 9:09 2002 Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Feb 27 11:30:15 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 23.31 168 79752 6.35 ug/1 # 91 31) 4-Bromophenyl-phenylether 24.39 248 49611 6.11 ug/1 98 32) Hexachlorobenzene 24.83 284 50878 5.35 ug/1 95 33) Phenanthrene 25.80 178 299239 7.72 ug/1 99 34) Anthracene 25.93 178 278345 7.33 ug/1 99 35) Di-n-butylphthalate 27.69 149 434543 8.02 ug/1 99 36) Fluoranthene 29.43 202 299996 7.75 ug/1 # 89 3 9) Pyrene 30.11 202 313491 7.89 ug/1 # 88 40) Butylbenzylphthalate 32.23 149 143616 6.53 ug/1 94 41) Benzo(a)anthracene 33.75 228 236678 8.15 ug/1 99 42) Bis(2-ethylhexyl)phthalate 34.01 149 212098 7.14 ug/1 95 43) Chrysene 33.87 228 252278 8.82 ug/1 100 45) Di-n-Octylphthalate 35.75 149 266224 5.40 ug/1 99 46) Benzo(b)fluoranthene 36.87 252 195914 7.04 ug/1 # 96 47) Benzo(k)fluoranthene 36.94 252 234942 8.40 ug/1 # 95 48) Benzo(a)pyrene 37.88 252 158049 6.85 ug/1 # 96 49) Indeno(1,2,3-cd)pyrene 42.29 276 179742 8.53 ug/1 # 92 50) Dibenz(a,h)anthracene 42.35 278 157861 9.81 ug/1 # 93 51) Benzo(g,h,i)perylene 43.55 276 165140 9.72 ug/1 # 93

(#) = qualifier out of range (m) = manual integration REFC2.D GCMS0208.M Fri Mar 08 09:12:15 2002 Page 2

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