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GCMS reference analysis results for VOCs, Feb 27 2002

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Laboratory report listing detection results for volatile organic compounds in reference sample AD31498 analyzed on February 27, 2002.

NYC-WTC_000038111–000038115

Folder label: “GCMS X 2/21/02 A 2/22/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\FEB21O2\REFB .D Vial: 31 Acq On : 22 Feb 2002 8:43 pm Operator: Sample : gc/ms scan 2/21 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 25 8:28 2002 Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Thu Feb 21 16:13:52 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 23.31 168 86951 5.73 ug/1 # 90 31) 4-Bromophenyl-phenylether 24.39 248 53962 5.50 ug/1 98 32) Hexachlorobenzene 24.83 284 62733 5.46 ug/1 96 3 3) Phenanthrene 25.80 178 308515 6.59 ug/1 99 3 4) Anthracene 25.93 178 293864 6.40 ug/1 99 35) Di-n-butylphthalate 27.69 149 419296 6.41 ug/1 99 36) Fluoranthene 29.43 202 296141 6.33 ug/1 # 88 3 9) Pyrene 30.11 202 306157 6.54 ug/1 # 88 40) Butylbenzylphthalate 32.23 149 155108 5.98 ug/1 93 41) Benzo(a)anthracene 33.75 228 226147 6.60 ug/1 99 42) Bis(2-ethylhexyl)phthalate 34.01 149 218050 6.23 ug/1 95 43) Chrysene 33.88 228 241898 7.18 ug/1 99 45) Di-n-Octylphthalate 35.75 149 258269 4.44 ug/1 99 46) Benzo(b)fluoranthene 36.87 252 188678 5.75 ug/1 # 96 47) Benzo(k)fluoranthene 36.94 252 217165 6.58 ug'/l # 95 4 8) Benzo(a)pyrene 37.88 252 158660 5.83 ug/1 # 95 49) Indeno(1,2,3-cd)pyrene 42.28 276 177264 7.14 ug/1 # 94 50) Dibenz(a,h)anthracene 42.35 278 148302 7.81 ug/1 # 94 51) Benzo(g,h,i)perylene 43.55 276 153447 7.66 ug/1 # 92

(#) = qualifier out of range (m) = manual integration REFB.D GCMS0208.M Wed Feb 27 11:15:04 2002 Page 2

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NYC-WTC_000038114Source: NYC Law Department, mirrored locally

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