GCMS calibration reference results, January 2002

NYC 9/11 Public Portal Document

? Quantitation Report (QT Reviewed) s” Data File : C:\HPCHEM\1\DATA\JAN2402\REFA.D Vial: 19 Acq On : 25 Jan 2002 4:45 am Operator: 209 GALOS Sample : GC/MS SCAN 1/2 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 14 11:55 2002 Quant Results File: GCMS0103.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Mon Jan 07 10:31:02 2002 Response via : Initial Calibration DataAcq Meth : GCMS0103

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.48 152 889120 20.00 ug/1 -0.05 10) Naphthalene-d8 15.08 136 3492801 20.00 ug/1 -0.04 17) Acenaphthene-diO 20.34 164 1742945 20.00 ug/1 -0.05 29) Phenanthrene-diO 24.76 188 2441435 20.00 ug/1 -0.05 38) Chrysene-dl2 32.78 240 1592695 20.00 ug/1 -0.06 44) Perylene-dl2 36.85 264 1069305 20.00 ug/1 -0.05

System Monitoring Compounds 37) 2,4-DDD 29.83 235 62948 2.25 ug/mL -0.24 Spiked Amount 5.000 Recovery = 45.00%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.27 74 38884 0.91 ug/1 96 3) bis(2-Chloroethyl)ether 10.92 93 99170 1.4 4ug/1 96 4) 1,3-Dichlorobenzene 11.39 146 51247 0.83 ug'/l 97 5) 1,4-Dichlorobenzene 11.53 146 58387m 0.94 ug/1 6) 1,2-Dichlorobenzene 12.04 146 57801 1.01 ug/1 98 7) 2,2’-oxybis(1-Chloropropan 12.39 45 168879 1.65 ug/1 96 8) N-Nitroso-di-n-propylamine 12.78 70 73511 1.71 ug/1 99 9) Hexachloroethane 12.87 117 14307 0.56 ug/1 96 11) Nitrobenzene 13.16 77 91372 1.36 ug/1 96 12) 1sophorone 13.81 82 201468 1.67 ug/1 98 13) bis(2-Chloroethoxy)methane 14.50 93 121735 1.56 ug/1 98 14) 1,2,4-Trichlorobenzene 14.98 180 47967 1.01 ug/1 98 15) Naphthalene 15.14 128 232263 1.45 ug/1 99 16) Hexachlorobutadiene 15.69 225 11775 0.49 ug/1 97 18) Hexachiorocyc1opentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 18.62 162 121430 1.34 ug/1 95 20) Dimethylphthalate 19.74 163 193180 1.83 ug/1 99 21) 2,6-Dinitrotoluene 19.95 165 28252 1.13 ug/1 93 22) Acenaphthylene 19.87 152 197112 1.48 ug/1 99 23) Ac enapht hene 20.43 153 147183 1.61 ug/1 99 24) 2,4-Dinitrotoluene 21.11 165 33322 1.04 ug/1 # 87 25) Diethylphthalate 21.86 149 198303 1.89 ug/1 98 26) 4-Chiorophenyl-phenylether 21.98 204 66961 1.57 ug/1 97 27) Fluorene 21.95 166 155724 1.68 ug/1 98 28) Azobenzen/ 1,2-Diphenylhyd 22.45 77 180714 1.45 ug/L 96

(#) = qualifier out of range (m) = manual integration REFA.D GCMS0103.M Thu Feb 14 11:55:45 2002 Page 1

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