GCMS calibration results, January 2002

NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\JANI6 0 2\CAL10.D Vial: 2 Acq On 16 Jan 2002 11:29 am Operator: 209 GALOS Sample Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 7 10:43 2002 Quant Results File: GCMS0103.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update ' : Mon Jan 07 10:31:02 2002 Response via : Initial Calibration DataAcq Meth : GCMS0103

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.51 152 738800 20.00 ug/1 -0.02 10) Naphthalene-d8 15.10 136 2840331 20.00 ug/1 -0.02 17) Acenaphthene-diO 20.36 164 1401760 20.00 ug/1 -0.03 29) Phenanthrene-diO 24.77 188 1924024 20.00 ug/1 -0.03 38) Chrysene-dl2 32.81 240 1183528 20.00 ug/1 -0.03 44) Perylene-dl2 36.86 264 725919 20.00 ug/1 -0.03

System Monitoring Compounds 37) 2,4-DDD 0.00 235 Od 0.00 ug/mL Spiked Amount 5.000 Recovery = 0.00%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.27 74 342498 9.66 ug/1 95 3) bis(2-Chloroethyl)ether 10.95 93 587266 10.26 ug/1 100 4) 1,3-Dichlorobenzene 11.40 146 529556 10.35 ug/1 100 5) 1,4-Dichlorobenzene 11.54 146 543736 10.55 ug/1 99 6) 1,2-Dichloroberizene 12.06 146 509451 10.70 ug/1 98 7) 2,21-oxybis(1-Chloropropan 12.40 45 887186 10.42 ug/1 96 8) N-Nitroso-di-n-propylamine 12.79 70 373238 10.45 ug/1 98 9) Hexachloroethane 12.88 117 217334 10.31 ug/1 98 11) Nitrobenzene 13.18 77 572792 10.45 ug/1 100 12) 1sophorone 13.82 82 1015768 10.38 ug/1 99 13) bis(2-Chloroethoxy)methane 14.52 93 651227 10.28 ug/1 100 14) 1,2,4-Trichlorobenzene 14.99 180 404390 10.46 ug/1 99 15) Naphthalene 15.15 128 1392759 10.71 ug/1 100 16) Hexachlorobutadiene 15.70 225 211501 10.81 ug/1 99 18) Hexachiorocyclopentadiene 17.88 237 44244 (4.49 ug/1 97 19) 2-Chloronaphthalene 18.63 162 768719 10.58 ug/1 99 . 20) Dimethylphthalate 19.75 163 891101 10.47 ug/1 100 21) 2,6-Dinitrotoluene 19.96 165 198880 9.86 ug/1 98 22) Acenaphthylene 19.89 152 1137501 10.64 ug/1 100 2 3) Acenaphthene 20.45 153 801968 10.92 ug/1 100 24) 2,4-Dinitrotoluene 21.12 165 245508 9.50 ug/1 # 88 25) Diethylphthalate 21.88 149 908905 10.76 ug/1- 99 26) 4-Chlorophenyl-phenylether 22.01 204 373406 10.90 ug/1 99 2 7) Fluorene 21.96 166 814035 10.93 ug/1 99 28) Azobenzen/ 1,2-Diphenylhyd 22.47 77 1017057 10.18 ug/L 99

(#) = qualifier out of range (m) = manual integration CALIO.D GCMS0103.M Thu Feb 07 10:44:02 2002 Page 1

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