GCMS calibration results, sample AD31432, Jan 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\l\DATA\JAN1802\CAL40.D Vial: 2 Acq On 18 Jan 2002 9:36 am Operator: 209 GALOS Sample Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 15 13:51 2002 Quant Results File: GCMS0103.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Mon Jan 07 10:31:02 2002 Response via : Initial Calibration DataAcq Meth : GCMS0103

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.51 152 1063431 20.00 ug/1 0.00 10) Naphthalene-d8 15.10 136 4063707 20.00 ug/1 0.00 17) Acenaphthene-diO 20.36 164 1999215 20.00 ug/1 0.00 29) Phenanthrene-diO 24.79 188 2891319 20.00 ug/1 0.00 38) Chrysene-dl2 32.82 240 1616752 20.00 ug/1 0.00 44) Perylene-dl2 36.87 264 904763 20.00 ug/1 0.00

System Monitoring Compounds 37) 2,4-DDD 0.00 235 Od 0.00 ug/mL Spiked Amount 5.000 Recovery = 0.00%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.27 74 2001212 39.22 ug/1 96 3) bis(2-Chloroethyl)ether 10.96 93 3141661 38.13 ug/1 99 4) 1,3-Dichlorobenzene 11.40 146 2970261 40.33 ug/1 100 5) 1,4-Dichlorobenzene 11.55 146 2970421 40.03 ug/1 99 6) 1,2-Dichlorobenzene 12.06 146 2722202 39.72 ug/1 99 7) 2,2’-oxybi s(1-Chioropropan 12.40 45 4778615 38.99 ug/1 96 8) N-Nitroso-di-n-propylamine 12.83 70 2054956 39.96 ug/1 99 9) Hexachioroethane 12.88 117 1249198 41.16 ug/1 99 11) Nitrobenzene 13.19 77 3112517 39.68 ug/1 99 12) 1sophorone 13.84 82 5640705 40.31 ug/1 99 13) bis(2-Chloroethoxy)methane 14.53 93 3606542 39.78 ug/1 99 14) 1,2,4-Trichlorobenzene 15.00 180 2228857 40.29 ug/1 99 15) Naphthalene 15.17 128 7433639 39.96 ug/1 100 16) Hexachiorobutadiene 15.71 225 1158886 41.40 ug/1 99 18) Hexachiorocyclopentadiene 17.87 237 618470 44.04 ug/1 97 19) 2-Chioronaphthalene 18.65 162 4200737 40.56 ug/1 99 20) Dimethylphthalate 19.77 163 4981657 41.03 ug/1 100 21) 2,6-Dinitrotoluene 19.99 165 1187507 41.26 ug/1 97 22) Acenaphthylene 19.90 152 6190209 40.59 ug/1 100 23) Acenaphthene 20.47 153 4239152 40.47 ug/1 99 24) 2,4-Dinitrotoluene 21.15 165 1521491 41.30 ug/1 93 25) Diethylphthalate 21.91 149 4989486 41.43 ug/1 99 26) 4-Chlorophenyl-phenylether 22.01 204 2019854 41.36 ug/1 98 27) Fluorene 21.99 166 4369216 41.13 ug/1 99 2 8) Azobenzen/ 1,2-Diphenylhyd 22.49 77 6045550 42.41 ug/L 99

(#) = qualifier out of range (m) = manual integration CAL40.D GCMS0208.M Fri Feb 15 13:52:19 2002 Page 1

NYC-WTC_0000 16547