GCMS reference analysis, sample AD31363, Jan-Feb 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\JAN1602\REF.D Vial: 5 Acq On : 16 Jan 2002 3:33 pm Operator: 209 GALOS Sample : gc/ms scan 12/27 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 7 8:14 2002 Quant Results File: GCMS0103.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Mon Jan 07 10:31:02 2002 Response via : Initial Calibration DataAcq Meth : GCMS0103

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.50 152 788679 20.00 ug/1 -0.03 10) Naphthalene-d8 15.09 136 3055344 20.00 ug/1 -0.03 17) Acenaphthene-diO 20.36 164 1530063 20.00 ug/1 -0.03 29) Phenanthrene-diO 24.77 188 2066105 20.00 ug/1 -0.04 38) Chrysene-dl2 32.80 240 1173022 20.00 ug/1 -0.04 44) Perylene-dl2 36.86 264 731847 20.00 ug/1 -0.04

System Monitoring Compounds 37) 2,4-DDD 29.85 235 143764 6.06 ug/mL -0.22 Spiked Amount 5.000 Recovery = 121.20%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.28 74 93168 2.46 ug/1 90 3) bis(2-Chloroethyl)ether 10.93 93 224045 3.67 ug/1 98 4) 1,3-Dichlorobenzene 11.40 146 111225 2.04 ug/1 99 5) 1,4-Dichlorobenzene 11.55 146 127260 2.31 ug/1 98 6) 1,2-Dichlorobenzene 12.05 146 133120 2.62 ug/1 99 7) 2,2'-oxybis(1-Chloropropan 12.40 45 377246 4.15 ug/1 95 8) N-Nitroso-di-n-propylamine 12.78 70 169189 4.44 ug/1 96 9) Hexachloroethane 12.88 117 30606 1.36 ug/1 97 11) Nitrobenzene 13.17 77 218884 3.71 ug/1 99 12) Isophorone 13.82 82 478727 4.55 ug/1 98 13) bis(2-Chloroethoxy)methane 14.51 93 277716 4.07 ug/1 99 14) 1,2,4-Trichlorobenzene 14.99 180 110212 2.65 ug/1 99 15) Naphthalene 15.15 128 529008 3.78 ug/1 100 16) Hexachlorobutadiene 15.70 225 24415 1.16 ug/1 99 18) Hexachlorocyclopentadiene 17.88 237 424 N.D. 19) 2-Chloronaphthalene 18.63 162 286863 3.62 ug/1 97 20) Dimethylphthalate 19.75 163 425561 4.58 ug/1 99 21) 2,6-Dinitrotoluene 19.96 165 77561 3.52 ug/1 98 22) Acenaphthylene 19.88 152 465694 3.99 ug/1 99 23) Ac enapht hene 20.44 153 336414 4.20 ug/1 99 24) 2,4-Dinitrotoluene 21.12 165 95799 3.40 ug/1 91 25) Diethylphthalate 21.88 149 440218 4.78 ug/1 99 26) 4-Chlorophenyl-phenylether 22.00 204 155896 4.17 ug/1 99 27) Fluorene 21.96 166 355901 4.38 ug/1 100 28) Azobenzen/ 1,2-Diphenylhyd 22.46 77 432688 3.97 ug/L 98

(#) = qualifier out of range (m) = manual integration REF.D GCMS0103.M Thu Feb 07 08:33:42 2002 Page 1

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