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GCMS reference analysis, sample AD31363, Jan-Feb 2002

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Reference analysis report for DEP sample AD31363 listing results for nitrosamines and chlorinated compounds from January 2002.

NYC-WTC_000016501–000016505

Folder label: “GCMS X 12/31/01 A 1/18/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\JAN1602\REF.D Vial: 5 Acq On : 16 Jan 2002 3:33 pm Operator: 209 GALOS Sample : gc/ms scan 12/27 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 7 8:14 2002 Quant Results File: GCMS0103.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Mon Jan 07 10:31:02 2002 Response via : Initial Calibration DataAcq Meth : GCMS0103

Compound R.T. QIon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 22.40 168 117761 3.48 ug/1 99 31) 4-Bromophenyl-phenylether 23.45 248 79939 4.15 ug/1 93 32) Hexachlorobenzene 23.87 284 92730 4.16 ug/1 96 3 3) Phenanthrene 24.83 178 480795 4.59 ug/1 99 34) Anthracene 24.97 178 428467 4.18 ug/1 99 35) Di-n-butylphthalate 26.80 149 746535 5.26 ug/1 99 36) Fluoranthene 28.44 202 438117 4.36 ug/1 97 39) Pyrene 29.11 202 456661 4.38 ug/1 96 40) Butylbenzylphthalate 31.29 149 219233 3.88 ug/1 94 41) Benzo(a)anthracene 32.75 228 282581 4.30 ug/1 99 42) Bis(2-ethylhexyl)phthalate 33.10 149 292011 3.82 ug/1 99 43) Chrysene 32.87 228 314529 4.87 ug/1 100 45) Di-n-Octylphthalate 34.85 149 297588 2.53 ug/1 # 94 46) Benzo(b)fluoranthene 35.83 252 212052 3.50 ug/1 98 47) Benzo(k)fluoranthene 35.88 252 298892 5.01 ug/1 100 4 8) Benzo(a)pyrene 36.70 252 153011 3.22 ug/1 96 49) Indeno(l,2,3-cd)pyrene 40.43 276 156701 3.49 ug/1 99 50) Dibenz(a,h)anthracene 40.48 278 135700 3.94 ug/1 97 51) Benzo(g,h,i)perylene 41.46 276 150177 4.01 ug/1 99

(#) = qualifier out of range (m) = manual integration REF.D GCMS0103.M Thu Feb 07 08:33:46 2002 Page 2

NYC-WTC_0000 16504

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NYC-WTC_000016504Source: NYC Law Department, mirrored locally

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