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GCMS calibration results for sample AE00005, Jan 24 2002

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Calibration report for GCMS analysis of sample AE00005 listing target compounds and response factors.

NYC-WTC_000050074–000050078

Folder label: “GCMS X 1/3/02 A 1/24/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\JAN2402\REF.D vial: 4 Acq On : 24 Jan 2002 3:59 pm Operator: 209 GALOS Sample : GC/MS SCAN 1/3 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 8 9:03 2002 Quant Results File: GCMS0103.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Mon Jan 07 10:31:02 2002 Response via : Initial Calibration DataAcq Meth : GCMS0103

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 22.39 168 106769 2.95 ug/1 99 31) 4-Bromophenyl-phenylether 23.44 248 66959 3.25 ug/1 95 32) Hexachlorobenzene 23.85 284 76681 3.22 ug/1 97 33) Phenanthrene 24.82 178 381515 3.40 ug/1 99 3 4) Anthracene 24.96 178 341284 3.11 ug/1 99 35) Di-n-butylphthalate 26.78 149 537995 3.54 ug/1 99 3 6) Fluoranthene 28.43 202 366508 3.41 ug/1 95 39) Pyrene 29.09 202 373334 2.90 ug/1 98 40) Butylbenzylphthalate 31.28 149 186482 2.67 ug/1 97 41) Benzo(a)anthracene 32.73 228 264401 3.26 ug/1 98 42) Bis(2-ethylhexyl)phthalate 33.09 149 281471 2.98 ug/1 99 43) Chrysene 32.85 228 280136 3.51 ug/1 100 45) Di-n-Octylphthalate 34.83 149 305567 1.88 ug/1 # 98 46) Benzo(b)fluoranthene 35.81 252 226601 2.71 ug/1 98 47) Benzo(k)fluoranthene 35.87 252 297230 3.62 ug/1 99 48) Benzo(a)pyrene 36.68 252 166932 2.55 ug/1 # 96 4 9) Indeno(1,2,3-cd)pyrene 40.39 276 188338 3.05 ug/1 94 50) Dibenz(a,h)anthracene 40.45 278 153140 3.23 ug/1 96 51) Benzo (g,h, Dperylene 41.43 276 180689 3.50 ug/1 97

(#) = qualifier out of range (m) = manual integration REF.D GCMS0103.M Fri Feb 08 09:06:01 2002 Page 2

NYC-WTC_000050077

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NYC-WTC_000050077Source: NYC Law Department, mirrored locally

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