GCMS calibration results for sample AE00005, Jan 24 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\JAN2402\REF.D Vial: 4 Acq On : 24 Jan 2002 3:59 pm Operator: 209 GALOS Sample : GC/MS SCAN 1/3 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 8 9:03 2002 Quant Results File: GCMS0103.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Mon Jan 07 10:31:02 2002 Response via : Initial Calibration DataAcq Meth : GCMS0103

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.49 152 826663 20.00 ug/1 -0.02 10) Naphthalene-d8 15.08 136 3193964 20.00 ug/1 -0.02 17) Acenaphthene-diO 20.35 164 1598895 20.00 ug/1 -0.02 29) Phenanthrene-diO 24.75 188 2211309 20.00 ug/1 -0.03 38) Chrysene-dl2 32.79 240 1448778 20.00 ug/1 -0.03 44) Perylene-dl2 36.84 264 1008163 20.00 ug/1 -0.02

System Monitoring Compounds 37) 2,4-DDD 29.84 235 119695 4.72 ug/mL 0.14 Spiked Amount 5.000 Recovery = 94.40%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.28 74 70973 1.79 ug/1 96 3) bis(2-Chloroethyl)ether 10.93 93 168934 2.64 ug/1 98 4) 1,3-Dichlorobenzene 11.39 146 113612 1.98 ug/1 97 5) 1,4-Dichlorobenzene 11.53 146 128021m 2.22 ug/1 6) 1,2-Dichlorobenzene 12.04 146 127368 2.39 ug/1 98 7) 2,2‘-oxybis(1-Chloropropan 12.39 45 286407 3.01 ug/1 95 8) N-Nitroso-di-n-propylamine 12.77 70 125159 3.13 ug/1 99 9) Hexachloroethane 12.87 117 32417 1.37 ug/1 95 11) Nitrobenzene 13.16 77 162528 2.64 ug/1 93 12) 1sophorone 13.81 82 346356 3.15 ug/1 100 13) bis(2-Chloroethoxy)methane 14.50 93 206743 2.90 ug/1 99 14) 1,2,4-Trichlorobenzene 14.98 180 105058 2.42 ug/1 98 15) Naphthalene 15.13 128 425213 2.91 ug/1 100 16) Hexachiorobutadiene 15.69 225 27316 1.24 ug/1 94 18) Hexachiorocyclopentadiene 17.87 237 240 N.D. 19) 2-Chloronaphthalene 18.61 162 239275 2.89 ug/1 98 20) Dimethylphthalate 19.73 163 332524 3.42 ug/1 99 21) 2,6-Dinitrotoluene 19.94 165 55721 2.42 ug/1 90 22) Acenaphthylene 19.87 152 360606 2.96 ug/1 98 23) Acenaphthene 20.43 153 268479 3.20 ug/1 100 24) 2,4-Dinitrotoluene 21.11 165 70320 2.39 ug/1 92 25) Diethylphthalate 21.86 149 337941 3.51 ug/1 99 26) 4-Chlorophenyl-phenylether 21.99 204 129535 3.32 ug/1 100 27) Fluorene 21.94 166 276070 3.25 ug/1 100 28) Azobenzen/ 1,2-Diphenylhyd 22.45 77 334296 2.93 ug/L 99

(#) = qualifier out of range (m) = manual integration REF.D GCMS0103.M Fri Feb 08 09:05:57 2002 Page 1

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