GCMS calibration results for sample AE00005, Jan 24 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\JAN24 02\CAL2 5.D Vial: 2 Acq On 24 Jan 2002 11:05 am Operator: 209 GALOS Sample Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 8 9:01 2002 Quant Results File: GCMS0103.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Mon Jan 07 10:31:02 2002 Response via : Initial Calibration DataAcq Meth : GCMS0103

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.49 152 653221 20.00 ug/1 -0.03 10) Naphthalene-d8 15.09 136 2559174 20.00 ug/1 -0.02 17) Acenaphthene-diO 20.35 164 1279590 20.00 ug/1 -0.02 29) Phenanthrene-diO 24.76 188 1860926 20.00 ug/1 -0.03 38) Chrysene-dl2 32.79 240 1310288 20.00 ug/1 -0.03 44) Perylene-dl2 36.84 264 788456 20.00 ug/1 -0.03

System Monitoring Compounds 37) 2,4-DDD 0.00 235 Od 0.00 ug/mL Spiked Amount 5.000 Recovery = 0.00%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.24 74 693230 22.12 ug/1 98 3) bis(2-Chloroethyl)ether 10.94 93 1185190 23.42 ug/1 100 4) 1,3-Dichlorobenzene 11.39 146 1080070 23.87 ug/1 100 5) 1,4-Dichlorobenzene 11.53 146 1090460 23.92 ug/1 98 6) 1,2-Dichlorobenzene 12.04 146 1034676 24.58 ug/1 99 7) 2,2'-oxybis(1-Chloropropan 12.39 45 1781184 23.66 ug/1 97 8) N-Nitroso-di-n-propylamine 12.78 70 751671 23.80 ug/1 99 9) Hexachloroethane 12.86 117 448221 24.04 ug/1 99 11) Nitrobenzene 13.17 77 1143117 23.14 ug/1 100 12) 1sophorone 13.81 82 2064794 23.43 ug/1 99 13) bis(2-Chloroethoxy)methane 14.51 93 1328007 23.26 ug/1 100 14) 1,2,4-Trichlorobenzene 14.98 180 837579 24.04 ug/1 100 15) Naphthalene 15.14 128 2872302 24.52 ug/1 100 16) Hexachiorobutadiene 15.69 225 449610 25.50 ug/1 99 18) Hexachlorocyclopentadiene 17.86 237 169651 18.88 ug/1 97 19) 2-Chloronaphthalene 18.62 162 1598205 24.11 ug/1 99 20) Dimethylphthalate 19.74 163 1874976 24.13 ug/1 100 21) 2,6-Dinitrotoluene 19.95 165 435024 23.62 ug/1 98 22) Acenaphthylene 19.88 152 2378077 24.36 ug/1 100 23) Acenapht hene 20.44 153 1648341 24.58 ug/1 100 24) 2,4-Dinitrotoluene 21.12 165 562377 23.85 ug/1 96 25) Diethylphthalate 21.88 149 1902206 24.68 ug/1 99 26) 4-Chlorophenyl-phenylether 21.99 204 786365 25.16 ug/1 100 27) Fluorene 21.95 166 1711254 25.17 ug/1 99 28) Azobenzen/ 1,2-Diphenylhyd 22.46 77 2156033 23.63 ug/L 99

(#) = qualifier out of range (m) = manual integration CAL25.D GCMS0103.M Fri Feb 08 09:01:34 2002 Page 1

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