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GCMS calibration results for sample AE00005, Jan 24 2002

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Laboratory report listing concentrations of volatile organic compounds in sample AE00005 used as a calibration standard.

NYC-WTC_000050070–000050073

Folder label: “GCMS X 1/3/02 A 1/24/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C: \HPCHEM\ 1 \DATA\JAN2 4 02 \ CAL2 5 . D Vial: 2 Acq On 24 Jan 2002 11:05 am Operator: 209 GALOS Sample Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 8 9:01 2002 Quant Results File: GCMS0103.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Mon Jan 07 10:31:02 2002 Response via : Initial Calibration DataAcq Meth : GCMS0103

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 22.39 168 728622 23.89 ug/1 99 31) 4-Bromophenyl-phenylether 23.45 248 422737 24.39 ug/1 100 32) Hexachlorobenzene 23.86 284 493049 24.58 ug/1 98 3 3) Phenanthrene 24.83 178 2294669 24.33 ug/1 100 3 4) Anthracene 24.96 178 2268691 24.58 ug/1 100 35) Di-n-butylphthalate 26.78 149 3206906 25.10 ug/1 100 3 6) Fluoranthene 28.43 202 2304165 25.46 ug/1 98 3 9) Pyrene 29.09 202 2367069 20.33 ug/1 99 40) Butylbenzylphthalate 31.29 149 1319500 20.90 ug/1 100 41) Benzo(a)anthracene 32.74 228 1728824 23.57 ug/1 99 42) Bis(2-ethylhexyl)phthalate 33.09 149 1843206 21.57 ug/1 100 43) Chrysene 32.87 228 1708569 23.69 ug/1 99 45) Di-n-Octylphthalate 34.83 149 2838709 22.36 ug/1 99 4 6) Benzo(b)fluoranthene 35.81 252 1362799 20.88 ug/1 100 47) Benzo(k)fluoranthene 35.88 252 1492881 23.24 ug/1 99 4 8) Benzo(a)pyrene 36.68 252 1229504 24.04 ug/1 97 49) Indeno(l,2,3-cd)pyrene 40.40 276 1190644 24.64 ug/1 96 50) Dibenz(a,h)anthracene 40.45 278 897771 24.22 ug/1 99 51) Benzo(g,h,i)perylene 41.44 276 998845m 24.77 ug/1

(#) = qualifier out of range (m) = manual integration CAL25.D GCMS0103.M Fri Feb 08 09:01:37 2002 Page 2

NYC-WTC_000050072

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NYC-WTC_000050072Source: NYC Law Department, mirrored locally

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