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GCMS calibration reference results, January 2002

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Gas chromatography-mass spectrometry calibration analysis documenting retention times and response values for deuterated reference standards from January 25, 2002.

NYC-WTC_000038119–000038121

Folder label: “GCMS X 2/21/02 A 2/22/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\JAN2402\REFA.D Vial: 19 Acq On : 25 Jan 2002 4:45 am Operator: 209 GALOS Sample : GC/MS SCAN 1/2 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 14 11:55 2002 Quant Results File: GCMS0103.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Mon Jan 07 10:31:02 2002 Response via : Initial Calibration DataAcq Meth : GCMS0103

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 22.39 168 54987 1.37 ug/1 96 31) 4-Bromophenyl-phenylether 23.44 248 35338 1.55 ug/1 96 3 2) Hexachlorobenzene 23.86 284 40618 1.54 ug/1 98 3 3) Phenanthrene 24.82 178 219835 1.78 ug/1 98 3 4) Anthracene 24.95 178 185169 1.53 ug/1 99 35) Di-n-butylphthalate 26.78 149 315598 1.88 ug/1 98 36) Fluoranthene 28.43 202 202235 1.70 ug/1 96 3 9) Pyrene 29.09 202 209046 1.48 ug/1 96 40) Butylbenzylphthalate 31.28 149 98958 1.29 ug/1 98 41) Benzo(a)anthracene 32.74 228 135552 1.52 ug/1 98 42) Bis(2-ethylhexyl)phthalate 33.09 149 136078 1.31 ug/1 99 43) Chrysene 32.85 228 147167 1.68 ug/1 99 45) Di-n-Octylphthalate 34.83 149 129452 0.75 ug/1 # 95 46) Benzo(b)fluoranthene 35.81 252 104234 1.18 ug/1 96 47) Benzo(k)fluoranthene 35.87 252 140533 1.61 ug/1 99 48) Benzo(a)pyrene 36.67 252 72979 1.05 ug/1 97 4 9) Indeno(1,2,3 -cd)pyrene 40.41 276 79031 1.21 ug/1 93 50) Dibenz(a,h)anthracene 40.46 278 58894 1.17 ug/1 94 51) Benzo(g,h,i)perylene 41.44 276 76860 1.41 ug/1 94

(#) = qualifier out of range (m) = manual integration REFA.D GCMS0103.M Thu Feb 14 11:55:48 2002 Page 2

NYC-WTC_000038120

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NYC-WTC_000038120Source: NYC Law Department, mirrored locally

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