Laboratory report of gas chromatography-mass spectrometry reference analysis performed on January 16, 2002.
NYC-WTC_000016280–000016284Folder label: “GCMS X 12/28/01 A 1/17/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File : C:\HPCHEM\1\DATA\JAN1602\REF.D Vial: 5 Acq On : 16 Jan 2002 3:33 pm Operator: 209 GALOS Sample : gc/ms scan 12/27 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 7 10:45 2002 Quant Results File: GCMS0103.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title ■ : 209 625/TCLP calibration table Last Update : Mon Jan 07 10:31:02 2002 Response via : Initial Calibration DataAcq Meth : GCMS0103
Compound R.T. Qlon Response Cone Unit Qvalue
30) N-Nitrosodiphenylamine 22.40 168 117761 3.48 ug/1 99 31) 4-Bromophenyl-phenylether 23.45 248 79939 4.15 ug/1 93 32) Hexachlorobenzene 23.87 284 92730 4.16 ug/1 96 33) Phenanthrene 24.83 178 480795 4.59 ug/1 99 34) Anthracene 24.97 178 428467 4.18 ug/1 99 35) Di -n-butylphthalate 26.80 149 746535 5.26 ug/1 99 36) Fluoranthene 28.44 202 438117 4.36 ug/1 97 3 9) Pyrene 29.11 202 456661 4.38 ug/1 96 40) Butylbenzylphthalate 31.29 149 219233 3.88 ug/1 94 41) Benzo(a)anthracene 32.75 228 282581 4.30 ug/1 99 42) Bis(2-ethylhexyl)phthalate 33.10 149 292011 3.82 ug/1 99 43) Chrysene 32.87 228 314529 4.87 ug/1 100 45) Di -n-Octylphthalate 34.85 14 9 297588 2.53 ug/1 # 94 46) Benzo(b)fluoranthene 35.83 252 212052 3.50 ug/1 98 47) Benzo(k)fluoranthene 35.88 252 298892 5.01 ug./1 100 48) Benzo(a)pyrene 36.70 2 52 15301.1 3.22 ug/1 96 49) Indeno(1,2,3-cd)pyrene 40.43 276 156701 3.49 ug/1 99 50) Dibenz(a,h)anthracene 40.48 278 135700 3.94 ug/1 97 51) Benzo(g,h,i)perylene 41.46 276 150177 4.01 ug/1 99
(#) = qualifier out of range (m) = manual integration REF.D GCMS0103.M Thu Feb 07 10:48:17 2002 Page 2
NYC-WTC_000016283
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NYC-WTC_000016550
Reference analysis report for DEP sample AD31432 listing results for volatile organic compounds from January 18, 2002.
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Reference analysis report for DEP sample AD31363 listing results for nitrosamines and chlorinated compounds from January 2002.
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GCMS reference analysis report for sample AD31129 listing component names and values from January 10, 2002.
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Analytical results for volatile organic compounds including nitrosamines and chlorinated benzenes.
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Reference standard analysis report verifying instrument performance for volatile organic compound testing in early 2002.
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Reference analysis report confirming instrument performance with measured values for nitrosamines and chlorinated solvents.
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Reference analysis report confirming instrument performance with measured values for nitrosamines and chlorinated solvents.
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Calibration report for GCMS analysis of sample AE00005 listing target compounds and response factors.
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Laboratory report of GCMS analysis of reference standards on February 28, 2002, verifying instrument performance.
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Reference standard analysis report for GCMS testing verifying instrument performance with specific compound concentrations on February 21, 2002.
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Reference standard analysis report for GCMS testing verifying instrument performance with specific compound concentrations.
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Reference standard analysis showing response factors for organic compounds from February 2002.
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NYC-WTC_000016550
Reference analysis report for DEP sample AD31432 listing results for volatile organic compounds from January 18, 2002.
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Calibration report for GCMS analysis of sample AE00005 listing target compounds and response factors.
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Gas chromatography-mass spectrometry calibration analysis documenting retention times and response values for deuterated reference standards from January 25, 2002.
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Reference analysis report for DEP sample AD31363 listing results for nitrosamines and chlorinated compounds from January 2002.
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Laboratory report listing concentrations of volatile organic compounds in sample AE00005 used as a calibration standard.
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Calibration report for DEP sample AD31432 listing response factors for volatile organic compounds from January 18, 2002.
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NYC-WTC_000016272
DEP GCMS analysis log covering samples processed between late December 2001 and mid-January 2002.
Filed in the same folder
NYC-WTC_000016273
Laboratory log sheet recording extraction parameters and sample processing details for GCMS analysis methods.
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NYC-WTC_000016276
Calibration results for GCMS analysis listing compounds and response factors from January 16, 2002.
Filed in the same folder
NYC-WTC_000016285
Laboratory report of a GCMS blank run performed on February 7, 2002, to verify absence of contamination.
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NYC-WTC_000016293
Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AD31401 conducted on February 11, 2002.
Filed in the same folder