GCMS calibration results, sample AD31432, Jan 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\JANI8 02\CAL40.D Vial: 2 Acq On 18 Jan 2002 9:36 am Operator: 209 GALOS Sample Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 15 13:51 2002 Quant Results File: GCMS0103.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Mon Jan 07 10:31:02 2002 Response via : Initial Calibration DataAcq Meth : GCMS0103

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 22.44 168 1887291 39.83 ug/1 96 31) 4-Bromophenyl-phenylether 23.47 248 1099494 40.83 ug/1 98 32) Hexachlorobenzene 23.90 284 1242489 39.86 ug/1 97 3 3) Phenanthrene 24.86 178 5842985 39.87 ug/1 99 3 4) Anthracene 25.00 178 5781910 40.32 ug/1 100 35) Di-n-butylphthalate 26.82 149 8264174 41.62 ug/1 100 36) Fluoranthene 28.47 202 5765493 41.01 ug/1 99 39) Pyrene 29.14 202 5816674 40.48 ug/1 97 40) Butylbenzylphthalate 31.31 149 3171196 40.71 ug/1 99 41) Benzo(a)anthracene 32.77 228 3704340 40.93 ug/1 99 42) Bis(2-ethylhexyl)phthalate 33.11 149 4238344 40.19 ug/1 100 43) Chrysene 32.90 228 3590176 40.35 ug/1 99 45) Di-n-Octylphthalate 34.86 149 6167713 42.34 ug/1 100 46) Benzo(b)fluoranthene 35.85 252 3048948 40.71 ug/1 99 47) Benzo(k)fluoranthene 35.91 252 3025660 41.04 ug/1 98 4 8) Benzo(a)pyrene 36.71 252 2480065 42.25 ug/1 100 49) Indeno(1,2,3-cd)pyrene 40.45 276 2491542 44.93 ug/1 99 50) Dibenz(a,h)anthracene 40.50 278 1943391 45.69 ug/1 99 51) Benzo(g,h,i)perylene 41.51 276 1976820m 42.71 ug/1

(#) = qualifier out of range (m) = manual integration CAL40.D GCMS0208.M Fri Feb 15 13:52:23 2002 Page 2

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