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GCMS calibration results, January 2002

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Calibration results for GCMS analysis listing compounds and response factors from January 16, 2002.

NYC-WTC_000016276–000016279

Folder label: “GCMS X 12/28/01 A 1/17/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\JANI6 02\CAL10.D Vial: 2 Acq On 16 Jan 2002 11:29 am Operator: 209 GALOS Sample Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 7 10:43 2002 Quant Results File: GCMS0103.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title ■: 209 625/TCLP calibration table Last Update ’ : Mon Jan 07 10:31:02 2002 Response via : Initial Calibration DataAcq Meth : GCMS0103

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 22.40 168 344637 10.93 ug/1 99 31) 4-Bromophenyl-phenylether 23.46 248 190947 10.66 ug/1 97 3 2) Hexachlorobenzene 23.87 284 233802 11.27 ug/1 97 3 3) Phenanthrene 24.84 178 1042508 10.69 ug/1 99 3 4) Anthracene 24.97 178 1009739 10.58 ug/1 99 35) Di-n-butylphthalate 26.80 149 1473672 11.15 ug/1 100 36) Fluoranthene 28.44 202 981122 10.49 ug/1 98 3 9) Pyrene 29.11 202 1003960 9.55 ug/1 99 40) Butylbenzylphthalate 31.30 149 534049 9.36 ug/1 98 41) Benzo(a)anthracene 32.75 228 654372 9.88 ug/1 99 42) Bis(2-ethylhexyl)phthalate 33.11 149 726227 9.41 ug/1 98 43) Chrysene 32.88 228 666205 10.23 ug/1 99 45) Di-n-Octylphthalate 34.84 149 916798 (7.84ug/l # 96 46) Benzo(b)fluoranthene 35.83 252 525317 8.74 ug/1 99 47) Benzo(k)fluoranthene 35.89 252 646585 10.93 ug/1 99 4 8) Benzo(a)pyrene 36.70 252 451652 9.59 ug'/l 98 49) Indeno(1,2,3-cd)pyrene 40.43 276 440449 9.90 ug/1 96 50) Dibenz(a,h)anthracene 40.48 278 337841 9.90 ug/1 98 51) Benzo(g,h,i)perylene 41.46 276 368705 9.93 ug/1 99

(#) = qualifier out of range (m) = manual integration CAL10.D GCMS0103.M Thu Feb 07 10:44:05 2002 Page 2

NYC-WTC_0000 16278

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NYC-WTC_000016278Source: NYC Law Department, mirrored locally

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