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GCMS reference results for sample AE01463, Feb 2002

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Reference data report for GCMS analysis of sample AE01463 conducted on February 27, 2002.

NYC-WTC_000003572–000003576

Folder label: “GCMS X 1/23/02 A 2/22/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

'Data File : C:\HPCHEM\l\DATA\FEB2102\REFA.D Vial: 17 Acq On : 22 Feb 2002 7:49 am Operator: Sample : gc/ms scan 1/22 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 26 14:05 2002 iQuant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Thu Feb 21 16:13:52 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 23.31 168 45049 2.69 ug/1 # 88 31) 4-Bromophenyl-phenylether 24.39 248 29786 2.75 ug/1 94 32) Hexachlorobenzene 24.82 284 34931 2.75 ug/1 99 33) Phenanthrene 25.80 178 165477 3.20 ug/1 99 34) Anthracene 25.93 178 147893 2.92 ug/1 99 35) Di-n-butylphthalate 27.70 149 227559 3.15 ug/1 99 36) Fluoranthene 29.42 202 151542 2.93 ug/1 # 87 39) Pyrene 30.10 202 158240 3.35 ug/1 # 87 40) Butylbenzylphthalate 32.23 149 65943 2.52 ug/1 95 41) Benzo(a)anthracene 33.75 228 105849 3.06 ug/1 100 42) Bis(2-ethylhexyl)phthalate 34.01 149 96591 2.73 ug/1 96 43) Chrysene 33.88 228 119395 3.51 ug/1 98 45) Di-n-Octylphthalate 35.75 149 99329 1.76 ug/1 # 98 46) Benzo(b)fluoranthene 36.87 252 83423 2.61 ug/1 # 94 47) Benzo(k)fluoranthene 36.93 252 104248 3.25 ug/1 # 93 48) Benzo(a)pyrene 37.88 252 63103 2.38 ug/1 # 93 49) Indeno(1,2,3-cd)pyrene 42.28 276 65839 2.73 ug/1 # 93 50) Dibenz(a,h)anthracene 42.36 278 56992 3.09 ug/1 # 90 51) Benzo(g,h,i)perylene 43.54 276 62002 3.18 ug/1 # 89

(#) = qualifier out of range (m) = manual integration REFA.D GCMS0208.M Tue Feb 26 14:07:46 2002 Page 2

NYC-WTC_000003575

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NYC-WTC_000003575Source: NYC Law Department, mirrored locally

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