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GCMS results for volatile organics sample AE01463, Feb 2002

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Laboratory report listing concentrations of volatile organic compounds in sample AE01463 analyzed on February 27, 2002.

NYC-WTC_000003568–000003571

Folder label: “GCMS X 1/23/02 A 2/22/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\FEB2102\CAL40A.D Vial: 2 Acq On : 22 Feb 2002 5:51 am Operator: Sample : gc/ms scan 1/22 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 26 12:34 2002 Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Thu Feb 21 16:13:52 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 23.34 168 665519 36.62 ug/1 # 87 31) 4-Bromophenyl-phenylether 24.40 248 379328 32.29 ug/1 96 32) Hexachlorobenzene 24.84 284 435441 31.68 ug/1 98 3 3) Phenanthrene 25.82 178 2029402 36.20 ug/1 99 34) Anthracene 25.95 178 2005333 36.51 ug/1 99 35) Di-n-butylphthalate 27.71 149 2664788 34.01 ug/1 99 36) Fluoranthene 29.45 202 2006393 35.85 ug/1 # 90 3 9) Pyrene 30.13 202 2019946 38.66 ug/1 # 88 40) Butylbenzylphthalate 32.24 149 1054795 36.46 ug/1 94 41) Benzo(a)anthracene 33.76 228 1433353 37.52 ug/1 99 42) Bis(2-ethylhexyl)phthalate 34.01 149 1306760 33.44 ug/1 96 43) Chrysene 33.90 228 1403182 37.33 ug/1 99 45) Di-n-Octylphthalate 35.76 149 1949212 32.22 ug/1 99 46) Benzo(b)fluoranthene 36.90 252 1205510 35.32 ug/1 # 97 47) Benzo(k)fluoranthene 36.97 252 1246726 36.34 ug/1 # 96 48) Benzo(a)pyrene 37.90 252 1097442 38.79 ug/1 # 94 49) Indeno(1,2,3-cd)pyrene 42.33 276 1067589 41.34 ug/1 # 91 50) Dibenz(a,h)anthracene 42.39 278 817330m 41.42 ug/1 51) Benzo(g,h,i)perylene 43.61 276 860563m 41.34 ug/1

(#) = qualifier out of range (m) = manual integration CAL40A.D GCMS0208.M Tue Feb 26 12:35:01 2002 Page 2

NYC-WTC_000003570

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NYC-WTC_000003570Source: NYC Law Department, mirrored locally

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