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GCMS calibration data, February 2002

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Calibration record for GCMS analysis conducted on February 28, 2002, listing response factors for target analytes.

NYC-WTC_000010158–000010161

Folder label: “GCMS X 1/25/02 A 2/25/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\FEB2502\CAL25.D Vial: 2 Acq On : 25 Feb 2002 11:40 am Operator: Sample : Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 28 8:56 2002 Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Feb 27 11:30:15 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 23.30 168 302396 22.56 ug/1 # 85 31) 4-Bromophenyl-phenylether 24.37 248 186139 21.48 ug/1 94 32) Hexachlorobenzene 24.81 284 226561 22.33 ug/1 # 91 3 3) Phenanthrene 25.79 178 969080 23.44 ug/1 99 34) Anthracene 25.92 178 941245 23.23 ug/1 99 35) Di-n-butylphthalate 27.68 149 1313099 22.72 ug/1 99 3 6) Fluoranthene 29.41 202 967808 23.44 ug/1 # 90 3 9) Pyrene 30.09 202 991797 24.82 ug/1 # 88 40) Butylbenzylphthalate 32.21 149 510296 23.06 ug/1 96 41) Benzo(a)anthracene 33.73 228 685047 23.44 ug/1 100 42) Bis(2-ethylhexyl)phthalate 33.98 149 696445 23.30 ug/1 97 43) Chrysene 33.86 228 685111 23.83 ug/1 99 45) Di-n-Octylphthalate 35.73 149 1034510 21.51 ug/1 99 46) Benzo(b)fluoranthene 36.85 252 606204 22.34 ug/1 # 96 47) Benzo(k)fluoranthene 36.92 252 602955 22.11 ug/1 # 96 48) Benzo(a)pyrene 37.86 252 520030 23.12 ug/1 # 96 49) Indeno(1,2,3-cd)pyrene 42.25 276 544660 26.53 ug/1 # 94 50) Dibenz(a,h)anthracene 42.32 278 407520 25.98 ug/1 # 93 51) Benzo(g,h,i)perylene 43.51 276 465703 28.14 ug/1 95

(#) = qualifier out of range (m) = manual integration CAL25.D GCMS0208.M Thu Feb 28 08:58:53 2002 Page 2

NYC-WTC_000010160

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NYC-WTC_000010160Source: NYC Law Department, mirrored locally

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