GCMS calibration analysis results, DEP Labs, Feb 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\FEB2 10 2\CAL4 0.D Vial: 2 Acq On 21 Feb 2002 2:06 pm Operator: Sample Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 22 8:36 2002 Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Thu Feb 21 16:13:52 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 23.34 168 604742 35.37 ug/1 # 84 31) 4-Bromophenyl-phenylether 24.40 248 377389 34.15 ug/1 95 32) Hexachlorobenzene 24.84 284 447296 34.56 ug/1 96 3 3) Phenanthrene 25.82 178 1945424 36.89 ug/1 99 34) Anthracene 25.95 178 1901691 36.80 ug/1 99 35) Di-n-butylphthalate 27.72 149 2628785 35.67 ug/1 # 99 3 6) Fluoranthene 29.45 202 1912828 36.33 ug/1 # 91 3 9) Pyrene 30.13 202 1961137 38.46 ug/1 # 90 40) Butylbenzylphthalate 32.24 149 1043241 36.95 ug/1 98 41) Benzo(a)anthracene 33.76 228 1398675 37.51 ug/1 99 42) Bis(2-ethylhexyl)phthalate 34.01 149 1321148 34.64 ug/1 96 43) Chrysene 33.90 228 1375303 37.49 ug/1 99 45) Di-n-Octylphthalate 35.76 149 1979496 32.32 ug/1 # 98 46) Benzo(b)fluoranthene 36.90 252 1207358 34.93 ug/1 # 97 47) Benzo(k)fluoranthene 36.97 252 1264787 36.41 ug/1 # 97 48) Benzo(a)pyrene 37.91 252 1087674 37.96 ug/1 # 95 49) Indeno(1,2,3-cd)pyrene 42.33 276 1132363m 43.31 ug/1 50) Dibenz(a,h)anthracene 42.39 278 885019 44.29 ug/1 # 94 51) Benzo(g,h,i)perylene 43.61 276 945037m 44.83 ug/1

(#) = qualifier out of range (m) = manual integration CAL40.D GCMS0208.M Fri Feb 22 08:37:19 2002 Page 2

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