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GCMS analysis results for sample AE02581, Mar 13, 2002

Machine-extracted title · confidence 90%

Laboratory report listing quantitative results for nitrosamines and chlorinated solvents in sample AE02581.

NYC-WTC_000005358–000005361

Folder label: “GCMS X 2/5/02 A 3/7/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\MAR0 7 0 2\CAL80.D Vial: 6 Acq On 7 Mar 2002 6:38 pm Operator: Sample Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 8 7:51 2002 Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Feb 27 11:30:15 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 23.33 168 2115430 64.78 ug/1 # 85 31) 4-Bromophenyl-phenylether 24.38 248 1235721 /62.09ug/1 91 32) Hexachlorobenzene 24.82 284 1391259 60.00 ug/1 95 3 3) Phenanthrene 25.80 178 6538266 63.20 ug/1 99 34) Anthracene 25.94 178 6555694 64.10 ug/1 99 35) Di-n-butylphthalate 27.69 149 8435015 ( 62.17 ug/1 99 36) Fluoranthene 29.44 202 7028313 66.41 ug/1 # 92 39) Pyrene 30.12 202 7093153 .87 ug/1 # 90 40) Butylbenzylphthalate 32.23 149 3833308 62.91ug/1 97 41) Benzo(a)anthracene 33.75 228 6013814 6742 ug/1 99 42) Bis(2-ethylhexyl)phthalate 33.99 149 5082142 60.91/ug/l 97 43) Chrysene 33.90 228 5750583 65.76 ug/1 99 45) Di-n-Octylphthalate 35.74 149 8870686 57.53 ug/1 # 98 46) Benzo(b)fluoranthene 36.88 252 6093440 65.64 ug/1 # 96 47) Benzo(k)fluoranthene 36.98 252 5401636 58.56 ug/1 # 97 48) Benzo(a)pyrene 37.91 252 5557530 69.31 ug/1 # 95 49) Indeno(l,2,3-cd)pyrene 42.36 276 7055935 82.97 ug/1 # 87 50) Dibenz(a,h)anthracene 42.45 278 5415890 81.26 ug/1 # 95 51) Benzo(g,h,i)perylene 43.67 276 5757419 85.10 ug/1 # 93

(#) = qualifier out of range (m) = manual integration CAL80.D GCMS0208.M Wed Mar 13 14:17:58 2002 Page 2

NYC-WTC_000005360

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NYC-WTC_000005360Source: NYC Law Department, mirrored locally

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