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GCMS calibration results, Sample AE04417, Mar 2002

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Laboratory report for GC/MS calibration analysis of sample AE04417 conducted on March 22, 2002.

NYC-WTC_000012305–000012308

Folder label: “GCMS X 3-1-02 A 3-21-02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\l\DATA\MAR2102\CAL40.D Vial: 2 Acq On 21 Mar 2002 12:15 pm Operator: Sample Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 22 8:35 2002 Quant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Mar 08 08:54:27 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 23.27 168 1020533 36.96 ug/1 # 81 31) 4-Bromophenyl-phenylether 24.32 248 617960 38.08 ug/1 94 3 2) Hexachlorobenzene 24.76 284 709017 37.63 ug/1 94 3 3) Phenanthrene 25.75 178 3269305 37.03 ug/1 99 34) Anthracene 25.88 178 3305646 37.75 ug/1 99 35) Di-n-butylphthalate 27.64 149 4059970 36.54 ug/1 99 36) Fluoranthene 29.37 202 3418901 36.91 ug/1 # 94 3 9) Pyrene 30.05 202 3480555 43.23 ug/1 # 93 40) Butylbenzylphthalate 32.17 149 1675578 40.36 ug/1 98 41) Benzo(a)anthracene 33.69 228 2515807 37.57 ug/1 99 42) Bis(2-ethylhexyl)phthalate 33.94 149 2123306 37.88 ug/1 95 43) Chrysene 33.82 228 2434132 37.07 ug/1 99 45) Di-n-Octylphthalate 35.69 149 3258582 41.42 ug/1 # 96 46) Benzo(b)fluoranthene 36.81 252 2105772 38.62 ug/1 97 47) Benzo(k)fluoranthene 36.88 252 2037292 38.32 ug/1 # 98 4 8) Benzo(a)pyrene 37.81 252 1853877 37.31 ug/1 # 96 49) Indeno(1,2,3-cd)pyrene 42.17 276 1938570 32.30 ug/1 # 95 50) Dibenz(a,h)anthracene 42.23 278 1516776 32.65 ug/1 96 51) Benzo(g,h,i)perylene 43.43 276 1578759 32.26 ug/1 96

(#) = qualifier out of range (m) = manual integration CAL40.D GCMS0308.M Fri Mar 22 08:39:01 2002 Page 2

NYC-WTC_000012307

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NYC-WTC_000012307Source: NYC Law Department, mirrored locally

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