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GCMS blank analysis results, April 2002

Machine-extracted title · confidence 95%

Laboratory report showing GCMS blank analysis for volatile organic compounds on April 2, 2002.

NYC-WTC_000058600–000058603

Folder label: “GCMS X 3/6/02 A 3/30/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\MAR3 002\CAL4 0.D Vial: 2 Acq On 29 Mar 2002 4:55 pm Operator: Sample Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 2 10:36 2002 Quant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Mar 29 10:31:28 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 23.25 168 1161722 38.51 ug/1 # 81 31) 4-Bromophenyl-phenylether 24.31 248 721170 40.68 ug/1 # 89 32) Hexachlorobenzene 24.75 284 842592 40.93 ug/1 # 87 3 3) Phenanthrene 25.73 178 3707734 38.44 ug/1 99 34) Anthracene 25.85 178 3619078 37.83 ug/1 99 35) Di-n-butylphthalate 27.62 149 4543496 37.43 ug/1 99 36) Fluoranthene 29.35 202 3744560 37.01 ug/1 95 39) Pyrene 30.02 202 3742274 49.25 ug/1 # 91 40) Butylbenzylphthalate 32.14 149 1677693 42.82 ug/1 97 41) Benzo(a)anthracene 33.66 228 2397682 37.94 ug/1 99 42) Bis(2-ethylhexyl)phthalate 33.91 149 1958274 37.02 ug/1 95 43) Chrysene 33.80 228 2300021 ‘ 37.11 ug/1 99 45) Di-n-Octylphthalate 35.66 149 2731711 45.23 ug/1 # 97 46) Benzo(b)fluoranthene 36.77 252 1801674m 43.04 ug/1 47) Benzo(k)fluoranthene 36.84 252 1806067 44.25 ug/1 # 97 48) Benzo(a)pyrene 37.77 252 1450475 38.02 ug/1 # 97 49) Indeno(1,2,3-cd)pyrene 42.09 276 1321470 28.68 ug/1 95 50) Dibenz(a,h)anthracene 42.17 278 1018226 2^-55 ug/1 97 51) Benzo(g,h,i)perylene 43.34 276 1047453 ug/1 96

(#) = qualifier out of range (m) = manual integration CAL40.D GCMS0308.M Tue Apr 02 10:37:39 2002 Page 2

NYC-WTC_000058602

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NYC-WTC_000058602Source: NYC Law Department, mirrored locally

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