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GCMS analysis results for sample AE01156, March 25 2002

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Laboratory report detailing GCMS analysis of environmental sample AE01156 conducted on March 25, 2002.

NYC-WTC_000059666–000059669

Folder label: “GCMS X 3/13/02 A 3/27/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\MAR210 2\CAL4 0A.D Vial: 2 Acq On 22 Mar 2002 9:57 am Operator: Sample Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 25 10:23 2002 Quant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Mar 08 08:54:27 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 23.27 168 1333440 36.45 ug/1 # 83 31) 4-Bromophenyl-phenylether 24.33 248 811648 37.76 ug/1 93 32) Hexachlorobenzene 24.77 284 939385 37.63 ug/1 94 3 3) Phenanthrene 25.75 178 4252823 36.36 ug/1 99 34) Anthracene 25.89 178 4249942 36.64 ug/1 99 35) Di-n-butylphthalate 27.64 149 5279302 35.86 ug/1 99 36) Fluoranthene 29.38 202 4506243 36.73 ug/1 # 93 39) Pyrene 30.06 202 4556146 41.85 ug/1 # 92 40) Butylbenzylphthalate 32.18 149 2197076 39.14 ug/1 97 41) Benzo(a)anthracene 33.69 228 3345962 36.95 ug/1 99 42) Bis(2-ethylhexyl)phthalate 33.94 149 2744155 36.20 ug/1 96 43) Chrysene 33.83 228 3219019 36.25 ug/1 99 45) Di-n-Octylphthalate 35.69 149 4148567 41.77 ug/1 # 98 46) Benzo(b)fluoranthene 36.81 252 2702143 39.26 ug/1 98 47) Benzo(k)fluoranthene 36.89 252 2772573 41.32 ug/1 # 97 48) Benzo(a)pyrene 37.82 252 2326319 37.09 ug/1 # 96 49) Indeno(1,2,3-cd)pyrene 42.18 276 2211940 29.20 ug/1 96 50) Dibenz(a,h)anthracene 42.24 278 1718300 29.30 ug/1 97 51) Benzo (g,.h, i) perylene 43.44 276 1759989 28.49 ug/1 96

(#) = qualifier out of range (m) = manual integration • CAL40A.D GCMS0308.M Mon Mar 25 10:27:43 2002 Page 2

\ NYC-WTC_000059668

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NYC-WTC_000059668Source: NYC Law Department, mirrored locally

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