GCMS analysis results for sample AE01156, March 25 2002

NYC 9/11 Public Portal Document

Quantitation lort (QT Reviewed)

Data File C:\HPCHEM\l\DATA\MAR2102\C ,4 0 .D Vial: 2 Acq On 22 Mar 2002 9:57 am Operator: Sample Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 25 10:23 2002 Quant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Mar 08 08:54:27 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.28 152 770013 20.00 ug/1 -0.08 10) Naphthalene-d8 15.92 136 3057786 20.00 ug/1 -0.08 17) Acenaphthene-dlO 21.23 164 1693850 20.00 ug/1 -0.09 29) Phenanthrene-dlO 25.68 188 2707932 20.00 ug/1 -0.09 38) Chrysene-dl2 33.75 240 1896118 20.00 ug/1 -0.10 44) Perylene-dl2 38.00 264 1127031 20.00 ug/1 -0.12

System Monitoring Compounds 37) 2,4-DDD 0.00 235 0 0.00 ug/mL Spiked Amount 5.000 Recovery = 0.00%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.92 74 994726 38.08 ug/1 # 71 3) bis(2-Chloroethyl)ether 11.70 93 1550792 36.87 ug/1 91 4) 1,3-Dichlorobenzene 12.17 146 1691420 38.91 ug/1 99 5) 1,4-Dichlorobenzene 12.32 146 1695613 38.92 ug/1 99 6) 1,2-Dichlorobenzene 12.84 146 1570943 38.66 ug/1 99 7) 2,2'-oxybis(1-Chloropropan 13.16 45 2112520 35.69 ug/1 99 8) N-Nitroso-di-n-propylamine 13.58 70 1046461 ■ 38.24 ug/1 # 87 9) Hexachloroethane 13.68 117 629765 38.67 ug/1 99 11) Nitrobenzene 13.98 77 1543124 36.92 ug/1 91 12) Isophorone 14.63 82 2947103 37.18 ug/1' 99 13) bis(2-Chloroethoxy)methane 15.30 93 1926698 37.14 ug/1 98 14) 1,2,4-Trichlorobenzene 15.81 180 1432174 39.90 ug/1 97 15) Naphthalene 15.98 128 4378982 38.74 ug/1 99 16) Hexachlorobutadiene 16.52 225 722889 _4iE_40 ug/1 99 18) Hexachlorocyclopentadiene 18.71 237 605102 52.75?uq/l 99 19) 2-Chloronaphthalene 19.49 162 2769792 158709 ug/1 97 20) Dimethylphthalate 20.59 163 3233247 37.93 ug/1 99 21) 2,6-Dinitrotoluene 20.81 165 790343 38.20 ug/1 # 79 '22) Acenaphthylene 20.76 152 3942026 37.92 ug/1 99 23) Acenaphthene 21.34 153 2752321 37.88 ug/1 98 24) 2,4-Dinitrotoluene 21.98 165 1054085 38.08 ug/1 # 77 25) Diethylphthalate 22.73 149 3109016 37.57 ug/1 95 26) 4-Chlorophenyl-phenylether 22.87 204 1396079 39.40 ug/1 92 27) Fluorene 22.85 166 2936313 38.21 ug/1 99 28) Azobenzen/ 1,2-Diphenylhyd 23.34 77 3036983 34.24 ug/L # 86

(#) = qualifier out of range (m) = manual integration CAL40A.D GCMS0308.M Mon Mar 25 10:27:39 2002 Page 1

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