Fragmented document page from DEP Box 23 archive, Mar 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\MAR2 2 0 2\CAL4 0A.D Vial: 2 Acq On 23 Mar 2002 9:51 am Operator: Sample Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 26 8:18 2002 Quant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Mar 08 08:54:27 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Internal Standards R.T. Qlon Response- Cone Units Dev (Min)

1) 1,4-Dichlorobenzene-d4 12.28 152 920375 20.00 ug/1 -0.07 10) Naphthalene-d8 15.92 136 3675376 20.00 ug/1 -0.07 17) Acenaphthene-diO 21.23 164 2000869 20.00 ug/1 -0.08 29) Phenanthrene-diO 25.68 188 3195071 20.00 ug/1 -0.08 38) Chrysene-dl2 33.75 240 2169164 20.00 ug/1 -0.09 44) Perylene-dl2 38.00 264 1278811 20.00 ug/1 -0.12

System Monitoring Compounds 37) 2,4-DDD 0.00 235 0 0.00 ug/mL Spiked Amount 5.000 Recovery = 0.00%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.93 74 1163015 37.25 ug/1 # 71 3) bis(2-Chloroethyl)ether 11.70 93 1856288 36.92 ug/1 91 4) 1,3-Dichlorobenzene 12.18 146 2013756 3 8.76ug'/l 100 5) 1,4-Dichlorobenzene 12.33 146 2016279 38.72 ug/1 99 6) 1,2-Dichlorobenzene 12.84 146 1871405 38.53 ug/1 100 7) 2,21-oxybis(1-Chloropropan 13.16 45 2518519 35.59 ug/1 99 8) N-Nitroso-di-n-propylamine 13.58 70 1244737 38.05 ug/1 # 86 9) Hexachloroethane 13.68 117 752600 38.67 ug/1 94 11) Nitrobenzene 13.99 77 1851891 36.86 ug/1 90 12) Isophorone 14.64 82 3516684 36.91 ug/1 99 13) bis(2-Chloroethoxy)methane 15.31 93 2294463 36.79 ug/1 98 14) 1,2,4-Trichlorobenzene 15.81 180 1707271 39.57 ug/1 97 15) Naphthalene 15.99 128 5236224 38.54 ug/1 99 16) Hexachlorobutadiene 16.51 225 878389 40.84 ug/1 99 18) Hexachlorocyclopentadiene 18.71 237 688752 —50.83 ug/l 99 19) 2-Chloronaphthalene 19.50 162 3296283 38.37 ug/1 97 20) Dimethylphthalate 20.60 163 3898844 38.72 ug/1 99 21) 2,6-Dinitrotoluene 20.82 165 949089 38.83 ug/1 # 79 22) Acenaphthylene 20.76 152 4681527 38.12 ug/1 99 23) Acenaphthene 21.33 153 3280064 38.21 ug/1 99 24) 2,4-Dinitrotoluene 21.98 165 1250334 38.24 ug/1 # 79 25) Diethylphthalate 22.74 149 3697454 37.83 ug/1 96 26) 4-Chlorophenyl-phenylether 22.87 204 1620851 38.72 ug/1 95 27) Fluorene 22.86 166 3431069 37.79 ug/1 99 28) Azobenzen/ 1,2-Diphenylhyd 23.34 77 3723044 35.54 ug/L # 86

(#) = qualifier out of range (m) = manual integration CAL40A.D GCMS0308.M Tue Mar 26 08:19:12 2002 Page 1

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