GCMS reference results, Sample AE04417, Mar 2002

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Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\MAR21O2\REF1.D Vial: 4 Acq On : 21 Mar 2002 2:14 pm Operator: Sample : gc/ms scan 3/1 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 22 8:42 2002 Quant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Mar 08 08:54:27 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.26 152 616590 20.00 ug/1 -0.09 10) Naphthalene-d8 15.91 136 2408588 20.00 ug/1 -0.09 17) Acenaphthene-diO 21.21 164 1288267 20.00 ug/1 -0.10 29) Phenanthrene-diO 25.67 188 1942789 20.00 ug/1 -0.10 38) Chrysene-dl2 33.73 240 1187892 20.00 ug/1 -0.12 44) Perylene-dl2 37.98 264 735966 20.00 ug/1 -0.14

System Monitoring Compounds 37) 2,4-DDD 30.73 235 68760 4.87 ug/mL 0.24 Spiked Amount 5.000 Recovery = 97.40%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.89 74 81434 3.89 ug/1 # 69 3) bis(2-Chloroethyl)ether 11.66 93 184666 5.48 ug/1 91 4) 1,3-Dichlorobenzene 12.16 146 123158 3.54 ug/1 100 5) 1,4-Dichlorobenzene 12.31 146 129969 3.73 ug/1 98 6) 1,2-Dichlorobenzene 12.82 146 131211 4.03 ug/1 98 7) 2,2'-oxybi s(1-Chloropropan 13.15 45 253922 5.36 ug/1 99 8) N-Nitroso-di-n-propylamine 13.53 70 129920 5.93 ug/1 # 85 9) Hexachloroethane 13.68 117 35064 2.69 ug/1 100 11) Nitrobenzene 13.94 77 171497 5.21 ug/1 94 12) 1sophorone 14.60 82 379315 6.07 ug/1 99 13) bis(2-Chloroethoxy)methane 15.28 93 229644 5.62 ug/1 98 14) 1,2,4-Trichlorobenzene 15.79 180 113726 4.02 ug/1 97 15) Naphthalene 15.96 128 448300 5.04 ug/1 100 16) Hexachlorobutadiene 16.51 225 28289 2.01 ug/1 97 18) Hexachlorocyclopentadiene 18.70 237 5012 0.57 ug/1 96 19) 2-Chloronaphthalene 19.47 162 273630 4.95 ug/1 96 20) Dimethylphthalate 20.55 163 405156 6.25 ug/1 99 21) 2,6-Dinitrotoluene 20.77 165 84079 5.34 ug/1 # 83 22) Acenaphthylene 20.74 152 461898 5.84 ug/1 98 23) Acenaphthene 21.31 153 310525 5.62 ug/1 98 24) 2,4-Dinitrotoluene 21.94 165 108909 5.17 ug/1 # 78 25) Diethylphthalate 22.69 149 391004 6.21 ug/1 95 26) 4-Chlorophenyl-phenylether 22.85 204 160888 5.97 ug/1 91 27) Fluorene 22.82 166 351522 6.01 ug/1 99 2 8) Azobenzen/ 1,2-Diphenylhyd 23.31 77 348164 5.16 ug/L # 88

(#) = qualifier out of range (m) = manual integration REFl.D GCMS0308.M Fri Mar 22 08:52:19 2002 Page 1

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