GCMS calibration data for sample AE04038, March 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\MAR22O2\REFA1.D Vial: 17 Acq On : 23 Mar 2002 11:49 am Operator : Sample : gc/ms scan 2/25 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 27 8:38 2002 Quant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue Mar 26 14:13:06 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.26 152 479805 20.00 ug/1 -0.09 10) Naphthalene-d8 15.91 136 1859782 20.00 ug/1 -0.09 17) Acenaphthene-diO 21.21 164 1020508 20.00 ug/1 -0.10 29) Phenanthrene-diO 25.66 188 1572014 20.00 ug/1 -0.11 38) Chrysene-dl2 33.73 240 1074135 20.00 ug/1 -0.12 44) Perylene-dl2 37.98 264 663003 20.00 ug/1 -0.14

System Monitoring Compounds $.07 37) 2,4-DDD 30.73 235 93733 T. 28" ug/mL 0.24 Spiked Amount 5.000 Recovery = 145.00% /0/7 Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.91 74 99221 6.10 ug/1 # 70 3) bis(2-Chloroethyl)ether 11.66 93 227358 8.67 ug/1 92 4) 1,3-Dichlorobenzene 12.16 146 188371 6.95 ug/1 98 5) 1,4 -Dichlorobe.nzene 12.31 146 198801 7.32 ug/1 99 6) 1,2-Dichlorobenzene 12.82 146 197.749 7.81 ug/1 99 7) 2,2'-oxybi s(1-Chloropropan 13.14 45 317281 8.60 ug/1 99 8) N-Nitroso-di-n-propylamine 13.53 70 156661 9.19 ug/1 # 86 9) Hexachloroethane 13.68 117 55555 5.48 ug/1 96 11) Nitrobenzene 13.94 77 206714 8.13 ug/1 92 12) 1sophorone 14.60 82 473899 9.83 ug/1 99 13) bis(2-Chloroethoxy)methane 15.27 93 280832 8.90 ug/1 98 14) 1,2,4-Trichlorobenzene 15.79 180 174229 7.98 ug/1 97 15) Naphthalene 15.96 128 614388 8.94 ug/1 99 16) Hexachlorobutadiene 16.50 225 53538 4.92 ug/1 97 18) Hexachlorocyclopentadiene 18.70 237 17440 2.52 ug/1 99 19) 2-Chloronaphthalene 19.47 162 391158 8.93 ug/1 95 20) Dimethylphthalate 20.55 163 511806 9.97 ug/1 99 21) 2,6-Dinitrotoluene 20.77 165 109138 8.76 ug/1 # 83 22) Acenaphthylene 20.74 152 595721 9.51 ug/1 99 2 3) Acenaphthene 21.31 153 410649 9.38 ug/1 99 24) 2,4-Dinitrotoluene 21.94 165 138741 8.32 ug/1 # 80 25) Diethylphthalate 22.69 149 496967 9.97 ug/1 95 26) 4-Chlorophenyl-phenylether 22.85 204 225896 10.58 ug/1 90 2 7) Fluorene 22.82 166 463291 10.01 ug/1 99 28) Azobenzen/ 1,2-Diphenylhyd 23.31 77 441239 8.26 ug/L # 86

(#) = qualifier out of range (m) = manual integration REFA1.D GCMS0308.M Wed Mar 27 08:44:38 2002 Page 1

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