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GCMS calibration data for sample AE04038, March 2002

Machine-extracted title · confidence 100%

Calibration record for GCMS analysis of sample AE04038 conducted on March 27, 2002, showing compound responses.

NYC-WTC_000011711–000011718

Folder label: “GCMS X 2/25/02 A 3/23/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\MAR22O2\REFA1.D Vial: 17 Acq On : 23 Mar 2002 11:4g am Operator : Sample : gc/ms scan 2/25 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 27 8:38 2002 Quant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 20g 625/TCLP calibration table Last Update : Tue Mar 26 14:13:06 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 23.23 168 176598 8.32 ug/1 # 81 31) 4-Bromophenyl-phenylether 24.32 248 121552 g.74 ug/1 # 90 32) Hexachlorobenzene 24.75 284 140988 g.73 ug/1 # gi­ 3 3) Phenanthrene 25.72 178 664733 9.79 ug/1 gs 34) Anthracene 25.86 178 621731 g.23 ug/1 98 35) Di-n-butylphthalate 27.62 149 830740 g.72 ug/1 gg 3 6) Fluoranthene 2g.35 202 676184 9.49 ug/1 # 93 3 g) Pyrene 30.03 202 700661 11.36 ug/1 # 92 40) Butylbenzylphthalate 32.16 149 307067 g.66 ug/1 98 41) Benzo(a)anthracene 33.67 228 490712 g.57 ug/1 98 42) Bis(2-ethylhexyl)phthalate 33.93 149 391784 g.12 ug/1 96 43) Chrysene 33.7g 228 511744 10.17 ug/1 gg 45) Di-n-Octylphthalate 35.67 149 500930 8.57 ug/1 # 97 46) Benzo(b)fluoranthene 36.77 252 384594 9.50 ug/1 98 47) Benzo(k)fluoranthene 36.85 252 434377 11.00 ug/1 98 4 8) Benzo(a)pyrene 37.78 252 276549 7.4g ug/1 # 97 4 g) Indeno(1,2,3 -cd)pyrene 42.11 276 325003 7.2g ug/1 95 50) Dibenz(a,h)anthracene 42.18 278 280248 8.12 ug/1 # 95 51) Benzo(g,h,i)perylene 43.35 276 277851 7.65 ug/1 94

(#) = qualifier out of range (m) = manual integration REFA1.D GCMS0308.M Wed Mar 27 08:44:42 2002 Page 2

NYC-WTC_000011714

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NYC-WTC_000011714Source: NYC Law Department, mirrored locally

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