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GCMS reference standard results, sample AE04948, March 2002

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Reference standard analysis for gas chromatography-mass spectrometry dated March 29, 2002.

NYC-WTC_000058727–000058734

Folder label: “GCMS X 3/7/02 A 3/27/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\MAR26O2\REFA1.D Vial: 19 Acq On : 27 Mar 2002 3:33 am Operator: Sample : gc/ms scan 3/7 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 29 11:15 2002 Quant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Mar 29 10:31:28 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 23.21 168 141570' 5.22 ug/1 # 81 31) 4-Bromophenyl-phenylether 24.29 248 97745 6.14 ug/1 # 90 32) Hexachlorobenzene 24.73 284 115225 6.23 ug/1 # 91 33) Phenanthrene 25.70 178 531032 6.13 ug/1 99 34) Anthracene 25.84 178 495890 5.77 ug/1 99 35) Di-n-butylphthalate 27.60 149 663664 6.09 ug/1 99 36) Fluoranthene 29.33 202 511199 5.62 ug/1 # 94 39) Pyrene 30.00 202 526928 8.33 ug/1 94 40) Butylbenzylphthalate 32.13 149 215652 6.61 ug/1 96 41) Benzo(a)anthracene 33.64 228 306654' 5.83 ug/1 99 42) Bis(2-ethylhexyl)phthalate 33.91 149 266755 6.05 ug/1 94 43) Chrysene 33.77 228 333091 6.45 ug/1 98 45) Di-n-Octylphthalate 35.65 149 294807 5.49 ug/1 # 98 46) Benzo(b)fluoranthene 36.75 252 243727 6.55 ug/1 99 47) Benzo(k)fluoranthene 36.82 252 252720 6.97 ug/1 97 48) Benzo(a)pyrene 37.74 252 167736 4.95 ug/1 98 49) Indeno(1,2,3-cd)pyrene 42.06 276 155043 3.79 ug/1 96 50) Dibenz(a,h)anthracene 42.13 278 130684 4.12 ug/1 96 51) Benzo(g,h,i)perylene 43.29 276 140381 4.20 ug/1 97

(#) = qualifier out of range (m) = manual integration REFAl.D GCMS0308.M Fri Mar 29 11:19:33 2002 Page 2

NYC-WTC_000058733

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NYC-WTC_000058733Source: NYC Law Department, mirrored locally

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