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GCMS reference standard results, sample AE04733, Apr 2002

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Reference standard analysis report for sample AE04733 conducted April 1, 2002, listing concentrations of quality control compounds.

NYC-WTC_000058258–000058265

Folder label: “GCMS X 3/4/02 A 3/23/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\MAR28O2\REF1.D Vial: 4 Acq On : 28 Mar 2002 11:29 am Operator: Sample : gc/ms scan 3/4 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 1 9:44 2002 Quant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Mar 29 10:31:28 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 23.22 168 123679 7.97 ug/1 # 78 31) 4-Bromophenyl-phenylether 24.29 248 83646 9.18 ug/1 93 32) Hexachlorobenzene 24.73 284 99034 9.36 ug/1 # 87 3 3) Phenanthrene 25.70 178 450183 9.08 ug/1 99 34) Anthracene 25.83 178 416215 8.46 ug/1 99 35) Di-n-butylphthalate 27.61 149 545638 8.74 ug/1 # 99 36) Fluoranthene 29.32 202 423683 8.14 ug/1 # 93 3 9) Pyrene 30.00 202 439366 12.15 ug/1 # 92 40) Butylbenzylphthalate 32.13 149 172453 9.25 ug/1 98 41) Benzo(a)anthracene 33.65 228 250204 8.32 ug/1 99 42) Bis(2-ethylhexyl)phthalate 33.91 149 212631 8.45 ug/1 95 43) Chrysene 33.77 228 282110 9.57 ug/1 98 45) Di-n-Octylphthalate 35.66 149 224372 7.36 ug/1 # 96 46) Benzo(b)fluoranthene 36.75 252 193196 9.14 ug/1 96 47) Benzo(k)fluoranthene 36.81 252 222683 10.81 ug/1 97 48) Benzo(a)pyrene 37.74 252 133815 6.95 ug/1 # 96 49) Indeno(l,2,3-cd)pyrene 42.06 276 122448 5.27 ug/1 99 50) Dibenz(a,h)anthracene 42.14 278 108384 6.02 ug/1 98 51) Benzo(g,h,i)perylene 43.30 276 111559 5.88 ug/1 96

{#) = qualifier out of range (m) = manual integration REFl.D GCMS0308.M Mon Apr 01 09:46:54 2002 Page 2

NYC-WTC_000058261

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NYC-WTC_000058261Source: NYC Law Department, mirrored locally

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