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GCMS calibration results, April 2002

Machine-extracted title · confidence 95%

Calibration data for GCMS analysis of volatile organic compounds recorded on April 2, 2002.

NYC-WTC_000058604–000058608

Folder label: “GCMS X 3/6/02 A 3/30/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\MAR3002\REF.D Vial: 5 Acq On : 29 Mar 2002 6:55 pm Operator: Sample : gc/ms scan 3/6 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 2 10:39 2002 Quant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Mar 29 10:31:28 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 23.21 168 159151 8.03 ug/1 # 79 31) 4-Bromophenyl-phenylether 24.30 248 104040 8.93 ug/1 # 88 32) Hexachlorobenzene 24.73 284 120327 8.89 ug/1 # 90 33) Phenanthrene 25.70 178 570462 9.00 ug/1 98 34) Anthracene 25.83 178 526286 8.37 ug/1 99 35) Di-n-butylphthalate 27.60 149 751873 9.42 ug/1 99 36) Fluoranthene 29.33 202 545703 8.21 ug/1 96 39) Pyrene 30.01 202 562284 12.12 ug/1 96 40) Butylbenzylphthalate 32.13 149 231029 9.66 ug/1 97 41) Benzo(a)anthracene 33.64 228 327504 8.49 ug/1 99 42) Bis(2-ethylhexyl)phthalate 33.91 149 275874 8.54 ug/1 94 43) Chrysene 33.77 228 355447 9.39 ug/1 ■ 100 45) Di-n-Octylphthalate 35.65 149 300968 7.83 ug/1 # 97 46) Benzo(b)fluoranthene 36.75 252 247380 9.28 ug/1 98 47) Benzo(k)fluoranthene 36.82 252 288771 11.12 ug/1 97 48) Benzo(a)pyrene 37.74 252 177992 7.33 ug/1 # 96 49) Indeno(1,2,3-cd)pyrene 42.05 276 168140 5.73 ug/1 95 50) Dibenz(a,h)anthracene 42.13 278 142418 6.27 ug/1 98 51) Benzo(g,h,i)perylene 43.29 276 148226 6.20 ug/1 95

(#) = qualifier out of range (m) = manual integration REF.D GCMS0308.M Tue Apr 02 10:42:13 2002 Page 2

NYC-WTC_000058607

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NYC-WTC_000058607Source: NYC Law Department, mirrored locally

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