Calibration results for specific volatile organic compounds used to verify GCMS instrument performance in April 2002.
NYC-WTC_000059118–000059125Folder label: “GCMS X 3/9/02 A 3/30/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File-: C:\HPCHEM\1\DATA\MAR3OO2\REFB2.D Vial: 41 Acq On : 31 Mar 2002 8:39 am Operator: Sample : gc/ms scan 3/9 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 3 13:40 2002 Quant Results File: GCMS0308.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Mar 29 10:31:28 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308
Compound R.T. Qlon Response Cone Unit Qvalue
30) N-Nitrosodiphenylamine 23.21 168 127273 6.80 ug/1 # 80 31) 4-Bromophenyl-phenylether 24.30 248 109748 9.98 ug/1 # 88 32) Hexachlorobenzene 24.73 284 132648 10.38 ug/1 # 90 ■ 33) Phenanthrene 25.70 178 572050 9.56 ug/1 99 34) Anthracene 25.83 178 515637 8.69 ug/1 98 35) Di-n-butylphthalate 27.60 149 757177 10.05 ug/1 99 36) Fluoranthene 29.33 202 560361 8.92 ug/1 96 39) Pyrene 30.00 202 569585 13.61 ug/1 # 92 40) Butylbenzylphthalate 32.13 149 242972 11.26 ug/1 99 41) Benzo(a)anthracene 33.64 228 324328 9.32 ug/1 99 42) Bis(2-ethylhexyl)phthalate 33.91 149 293037 10.06 ug/1 93 43) Chrysene 33.76 228 353379 10.35 ug/1 99 45) Di-n-Octylphthalate 35.65 149 325404 8.99 ug/1 # 96 46) Benzo(b)fluoranthene 36.74 252 255473 10.18 ug/1 98 47) Benzo(k)fluoranthene 36.81 252 273185m 11.17 ug/1 48) Benzo(a)pyrene 37.74 252 170822 7.47 ug/1 # 97 49) Indeno(1,2,3-cd)pyrene 42.05 276 171147 6.20 ug/1 95 50) Dibenz(a,h)anthracene 42.12 278 149503 7.00 ug/1 98 51) Benzo(g,h,i)perylene 43.29 276 156177 6.94 ug/1 97
(#) = qualifier out of range (m) = manual integration REFB2.D GCMS0308.M Wed Apr 03 13:41:09 2002 Page 2
NYC-WTC_000059121
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NYC-WTC_000058911
Quantitative results for reference standards analyzed by GCMS on April 3, 2002, to validate analytical accuracy.
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Laboratory report showing GCMS calibration analysis for volatile organic compounds on April 2, 2002.
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Laboratory report listing concentrations of target analytes in a reference standard analyzed on March 29, 2002.
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Reference standard analysis for gas chromatography-mass spectrometry dated March 29, 2002.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000059491
Calibration data sheet listing retention times and response factors for multiple organic compounds analyzed on April 5, 2002.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000058175
Analysis of reference standards for nitrosamines and VOCs with measured concentrations near target levels on March 29, 2002.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000059222
Reference standard analysis report for volatile organic compounds using GCMS on April 4, 2002.
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Reference standard analysis report for sample AE04733 conducted April 1, 2002, listing concentrations of quality control compounds.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000058498
Laboratory report listing concentrations of target analytes in a reference standard analyzed on April 2, 2002.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000011849
Reference analysis record for GCMS testing of sample AE04388 conducted on March 28, 2002, by analyst MG.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000011711
Calibration record for GCMS analysis of sample AE04038 conducted on March 27, 2002, showing compound responses.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010289
Reference data report displaying measured concentrations and detection limits for target analytes analyzed on March 21, 2002.
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Laboratory report showing non-detect levels for various organic compounds in a GCMS blank sample from April 2002.
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Calibration results for specific volatile organic compounds used to verify GCMS instrument performance in April 2002.
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Laboratory report documenting GCMS analysis of sample AE05231 for unknown compounds on April 9, 2002.
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