GCMS reference analysis results, sample AE05231, April 2002

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Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\MAR3OO2\REFB2.D Vial: 41 Acq On : 31 Mar 2002 8:39 am Operator: Sample : gc/ms scan 3/9 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 3 13:40 2002 Quant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri M^r 29 10:31:28 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.25 152 461126 20.00 ug/1 -0.10 10) Naphthalene-d8 15.89 136 1697524 20.00 ug/1 -0.11 17) Acenaphthene-dlO 21.19 164 968233 20.00 ug/1 -0.12 29) Phenanthrene-dlO 25.64 188 1385666 20.00 ug/1 -0.13 38) Chrysene-dl2 33.70 240 729014 20.00 ug/1 -0.15 44) Perylene-dl2 37.94 264 410781 20.00 ug/1 -0.18

System Monitoring Compounds 37) 2,4-DDD 30.70 235 88428 6.36 ug/mL 0.21 Spiked Amount 5.000 Recovery = 127.20%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.89 74 75703 4.84 ug/1 # 70 3) bis(2-Chloroethyl)ether 11.65 93 192610 7.65 ug/1 89 4) 1,3-Dichlorobenzene 12.15 146 160731 6.17 ug/1 97 5) 1,4-Dichlorobenzene 12.30 146 168516 6.46 ug/1 100 6) 1,2-Dichlorobenzene 12.81 146 165945 6.82 ug/1 98 7) 2,2'-oxybis(1-Chloropropan 13.12 45 266080 7.51 ug/1 99 , 8) N-Nitroso-di-n-propylamine 13.51 70 121473 7.41 ug/1 # 88 9) Hexachloroethane 13.66 117 49958 5.12 ug/1 100 11) Nitrobenzene 13.93 77 175176 7.55 ug/1 92 12) Isophorone 14.57 82 387537 8.81 ug/1 99 13) bis(2-Chloroethoxy)methane 15.25 93 235297 8.17 ug/1 98 14) 1,2,4-Trichlorobenzene 15.77 180 149490 7.50 ug/1 98 15) Naphthalene 15.94 128 527751 8.41 ug/1 99 16) Hexachlorobutadiene 16.48 225 56073 5.64 ug/1 97 18) Hexachlorocyclopentadiene 18.68 237 19253 2.94 ug/1 99 19) 2-Chloronaphthalene 19.45 162 326223 7.85 ug/1 96 20) Dimethylphthalate 20.53 163 476556 9.78 ug/1 99 21) 2,6-Dinitrotoluene 20.75 165 93365 7.89 ug/1 # 80 22) Acenaphthylene 20.72 152 505054 8.50 ug/1 99 23) Acenaphthene 21.28 153 358494 8.63 ug/1 98 24) 2,4-Dinitrotoluene 21.92 165 118552 7.49 ug/1 # 74 25) Diethylphthalate 22.67 149 461903 9.77 ug/1 # 94 26) 4-Chlorophenyl-phenylether 22.83 204 199312 9.84 ug/1 89 27) Fluorene 22.80 166 403668 9.19 ug/1 100 28) Azobenzen/ 1,2-Diphenylhyd 23.29 77 376972 7.44 ug/L # 84

(#) = qualifier out of range (m) = manual integration REFB2.D GCMS0308.M Wed Apr 03 13:41:06 2002 Page 1

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