GCMS reference standard results, sample AE04733, Apr 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\MAR28O2\REF1.D Vial: 4 Acq On : 28 Mar 2002 11:29 am Operator: Sample : gc/ms scan 3/4 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 1 9:44 2002 Quant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Mar 29 10:31:28 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) l,4-Dichlorobenzene-d4 12.25 152 383966 20.00 ug/1 -0.11 10) Naphthalene-d8 15.89 136 1412733 20.00 ug/1 -0.11 17) Acenaphthene-dlO 21.19 164 801722 20.00 ug/1 -0.12 29) Phenanthrene-dlO 25.64 188 1148081 20.00 ug/1 -0.13 38) Chrysene-dl2 33.70 240 629584 20.00 ug/1 -0.14 44) Perylene-dl2 37.94 264 345968 20.00 ug/1 -0.18

System Monitoring Compounds 37) 2,4-DDD 30.71 235 59201 5.14 ug/mL 0.21 Spiked Amount 5.000 Recovery = 102.80%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.89 74 74038 5.68 ug/1 # 72 3) bis(2-Chloroethyl)ether 11.64 93 177662 8.47 ug/1 92 4) 1,3-Dichlorobenzene 12.15 146 126713 5.85 ug/1 98 5) 1,4-Dichlorobenzene 12.29 146 133513 6.15 ug/1 99 6) 1,2-Dichlorobenzene 12.82 146 135142 6.67 ug/1 97 7) 2,2'-oxybis(1-Chloropropan 13.13 45 245694 8.32 ug/1 98 8) N-Nitroso-di-n-propylamine 13.51 70 115781 8.48 ug/1 # 86 9) Hexachloroethane 13.66 117 35539 4.38 ug/1 95 11) Nitrobenzene 13.93 77 154581 8.00 ug/1 93 12) Isophorone 14.58 82 342123 9.34 ug/1 98 13) bis(2-Chloroethoxy)methane 15.26 93 210518 8.78 ug/1 97 14) 1,2,4-Trichlorobenzene 15.77 180 117162 7.07 ug/1 96 15) Naphthalene 15.95 128 452144 8.66 ug/1 99 16) Hexachlorobutadiene 16.49 225 36193 4.38 ug/1 ■ 97 18) Hexachlorocyclopentadiene 18.68 237 12642 2.33 ug/1 95 19) 2-Chloronaphthalene 19.44 162 269738 7.84 ug/1 96 20) Dimethylphthalate 20.54 163 361929 8.97 ug/1 99 21) 2,6-Dinitrotoluene 20.75 165 70205 7.17 ug/1 # 84 22) Acenaphthylene 20.72 152 423921 8.61 ug/1 100 23) Acenaphthene 21.28 153 293937 8.55 ug/1 97 24) 2,4-Dinitrotoluene 21.92 165 85609 6.53 ug/1 # 74 25) Diethylphthalate 22.67 149 344802 8.80 ug/1 94 26) 4-Chlorophenyl-phenylether 22.82 204 156160 9.31 ug/1 91 27) Fluorene 22.80 166 322273 8.86 ug/1 99 2 8) Azobenzen/ 1,2-Diphenylhyd 23.29 77 294085 7.01 ug/L # 85

(#) = qualifier out of range (m) = manual integration REFl.D GCMS0308.M Mon Apr 01 09:46:51 2002 Page 1

NYC-WTC_000058260