GCMS reference standard results for sample AE04590

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Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\MAR2602\REF.D Vial: 4 Acq On : 26 Mar 2002 11:41 am Operator: Sample : gc/ms scan 3/4 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 28 15:13 2002 Quant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Mar 08 08:54:27 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.25 152 622134 20.00 ug/1 -0.10 10) Naphthalene-d8 15.89 136 2375989 20.00 ug/1 -0.10 17) Acenaphthene-dlO 21.20 164 1292051 20.00 ug/1 -0.11 29) Phenanthrene-dlO 25.64 188 1896032 20.00 ug/1 -0.12 38) Chrysene-dl2 33.70 240 1060616 20.00 ug/1 -0.14 44) Perylene-dl2 37.94 264 608689 20.00 ug/1 -0.18

System Monitoring Compounds 37) 2,4-DDD 30.71 235 93493 ug/mL 0.21 Spiked Amount 5.000 Recovery

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.90 74 91584 4.34 ug/1 # 70 3) bis(2-Chloroethyl)ether 11.64 93 211783 6.23 ug/1 91 4) 1,3-Dichlorobenzene 12.15 146 172208 4.90 ug/1 99 5) 1,4-Dichlorobenzene 12.30 146 178971 5.08 ug/1 99 6) 1,2-Dichlorobenzene 12.81 146 180737 5.50 ug/1 99 7) 2,2'-oxybis(1-Chloropropan 13.13 45 296583 6.20 ug/1 98 8) N-Nitroso-di-n-propylamine 13.52 70 140831 6.37 ug/1 # 86 9) Hexachloroethane 13.66 117 50847 3.86 ug/1 94 11) Nitrobenzene 13.93 77 192439 5.92 ug/1 93 12) Isophorone 14.58 82 430298 6.99 ug/1 99 13) bis(2-Chloroethoxy)methane 15.26 93 259725 6.44 ug/1 98 14) 1,2,4-Trichlorobenzene 15.77 180 160320 5.75 ug/1 96 15) Naphthalene 15.95 128 578475 6.59 ug/1 99 16) Hexachlorobutadiene 16.49 225 54096 3.89 ug/1 99 18) Hexachlorocyclopentadiene 18.68 237 23645 2.70 ug/1 99 19) 2-Chloronaphthalene 19.45 162 364819 6.58 ug/1 96 20) Dimethylphthalate 20.54 163 508190 7.82 ug/1 99 21) 2,6-Dinitrotoluene 20.75 165 105520 6.69 ug/1 # 84 22) Acenaphthylene 20.72 152 562007 7.09 ug/1 99 23) Acenaphthene 21.28 153 400761 7.23 ug/1 98 24) 2,4-Dinitrotoluene 21.93 165 134067 6.35 ug/1 # 74 25) Diethylphthalate 22.67 149 491701 7.79 ug/1 95 26) 4-Chlorophenyl-phenylether 22.82 204 219946 8.14 ug/1 90 27) Fluorene 22.81 166 451572 7.70 ug/1 100 28) Azobenzen/ 1,2-Diphenylhyd 23.29 77 412961 6.10 ug/L # 83

(#) = qualifier out of range (m) = manual integration REF.D GCMS0308.M Thu Mar 28 15:14:34 2002 Page 1

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