GCMS reference standard results, sample AE04733, Apr 2002

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Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\MAR28O2\REF2.D Vial: 5 Acq On : 28 Mar 2002 12:29 pm Operator : Sample : gc/ms scan 3/4 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 1 9:47 2002 Quant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Mar 29 10:31:28 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) l,4-Dichlorobenzene-d4 12.25 152 417736 20.00 ug/1 -0.10 10) Naphthalene-d8 15.89 136 1523937 20.00 ug/1 -0.11 17) Acenaphthene-dlO 21.19 164 859806 20.00 ug/1 -0.12 29) Phenanthrene-dlO 25.64 188 1249430 20.00 ug/1 -0.13 38) Chrysene-dl2 33.70 240 670646 20.00 ug/1 -0.15 44) Perylene-dl2 37.94 264 364721 20.00 ug/1 -0.18

System Monitoring Compounds 37) 2,4-DDD 30.71 235 73273 5.85 ug/mL 0.21 Spiked Amount 5.000 Recovery = 117.00%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.89 74 84700 5.98 ug/1 # 71 3) bis(2-Chloroethyl)ether 11.64 93 210734 9.23 ug/1 90 4) 1,3-Dichlorobenzene 12.15 146 146317 6.20 ug/1 98 5) 1,4-Dichlorobenzene 12.30 146 157599 6.67 ug/1 97 6) 1,2-Dichlorobenzene 12.81 146 160790 7.29 ug/1 99 7) 2,2'-oxybis(1-Chloropropan 13.13 45 289738 9.02 ug/1 98 8) N-Nitroso-di-n-propylamine 13.52 70 138738 9.34 ug/1 # 85 9) Hexachloroethane 13.66 117 37723 4.27 ug/1 96 11) Nitrobenzene 13.93 77 188286 9.04 ug/1 90 12) Isophorone 14.57 82 415015 10.50 ug/1 100 13) bis(2-Chloroethoxy)methane 15.26 93 252053 9.75 ug/1 97 14) 1,2,4-Trichlorobenzene 15.78 180 141041 7.88 ug/1 95 15) Naphthalene 15.94 128 533753 9.48 ug/1 99 16) Hexachlorobutadiene 16.49 225 32465 3.64 ug/1 97 18) Hexachlorocyclopentadiene 18.69 237 13826 2.37 ug/1 93 19) 2-Chloronaphthalene 19.45 162 325815 8.83 ug/1 96 20) Dimethylphthalate 20.54 163 437652 10.12 ug/1 99 21) 2,6-Dinitrotoluene 20.75 165 90501 8.62 ug/1 # 80 22) Acenaphthylene 20.72 152 506379 9.60 ug/1 100 23) Acenaphthene 21.28 153 357398 9.69 ug/1 98 24) 2,4-Dinitrotoluene 21.92 165 108266 7.71 ug/1 # 78 25) Diethylphthalate 22.67 149 421451 10.03 ug/1 94 26) 4-Chlorophenyl-phenylether 22.83 204 188485 10.48 ug/1 92 2 7) Fluorene 22.81 166 394862 10.12 ug/1 100 2 8) Azobenzen/ 1,2-Diphenylhyd 23.29 77 364087 8.09 ug/L # 81

(#) = qualifier out of range (m) = manual integration REF2.D GCMS0308.M Mon Apr 01 09:50:01 2002 Page 1

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