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GCMS reference standard results, sample AE04733, Apr 2002

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Reference standard analysis report for sample AE04733 conducted April 1, 2002, listing concentrations of quality control compounds.

NYC-WTC_000058258–000058265

Folder label: “GCMS X 3/4/02 A 3/23/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\MAR28O2\REF2.D Vial: 5 Acq On : 28 Mar 2002 12:29 pm Operator: Sample : gc/ms scan 3/4 Inst ; GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 1 9:47 2002 Quant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Mar 29 10:31:28 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Compound R.T. QIon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 23.21 168 145211 8.60 ug/1 # 82 31) 4-Bromophenyl-phenylether 24.30 248 100511 10.13 ug/1 # 90 3 2) Hexachlorobenzene 24.73 284 119041 10.34 ug/1 91 3 3) Phenanthrene 25.70 178 545052 10.10 ug/1 99 34) Anthracene 25.84 178 509818 9.53 ug/1 99 35) Di-n-butylphthalate 27.60 149 675057 9.94 ug/1 99 36) Fluoranthene 29.33 202 516983 9.13 ug/1 # 94 3 9) Pyrene 30.01 202 536430 13.93 ug/1 95 40) Butylbenzylphthalate 32.14 149 220209 11.09 ug/1 96 41) Benzo(a)anthracene 33.64 228 297266 9.28 ug/1 99 42) Bis(2-ethylhexyl)phthalate 33.91 149 269930 10.07 ug/1 96 43) Chrysene 33.77 228 326689 10.40 ug/1 99 45) Di-n-Octylphthalate 35.65 149 298148 9.28 ug/1 # 97 46) Benzo(b)fluoranthene 36.75 252 222125 9.97 ug/1 97 47) Benzo(k)fluoranthene 36.82 252 240440 11.07 ug/1 98 48) Benzo(a)pyrene 37.74 252 154640 7.62 ug/1 # 97 49) Indeno(1,2,3-cd)pyrene 42.06 276 156485 6.38 ug/1 95 50) Dibenz(a,h)anthracene 42.13 278 131173 6.91 ug/1 97 51) Benzo(g,h,i)perylene 43.29 276 138312 6.92 ug/1 95

(#) = qualifier out of range (m) = manual integration REF2.D GCMS0308.M Mon Apr 01 09:50:05 2002 Page 2

NYC-WTC_000058264

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NYC-WTC_000058264Source: NYC Law Department, mirrored locally

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