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GCMS reference data for sample AE04388, March 2002

Machine-extracted title · confidence 100%

Reference analysis record for GCMS testing of sample AE04388 conducted on March 28, 2002, by analyst MG.

NYC-WTC_000011849–000011856

Folder label: “GCMS X 2/28/02 A 3/26/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\MAR2502\REF2A.D Vial: 11 Acq On : 25 Mar 2002 8:04 pm Operator: Sample : gc/ms scan 2/28 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 28 11:12 2002 Quant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue Mar 26 14:13:06 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 23.21 168 176819 8.98 ug/1 # 79 31) 4-Bromophenyl-phenylether 24.30 248 123640 10.68 ug/1 # 88 32) Hexachlorobenzene 24.73 284 133636 9.94 ug/1 # 89 3 3) Phenanthrene 25.70 178 683264 10.85 ug/1 99 34) Anthracene 25.83 178 631804 10.12 ug/1 98 35) Di-n-butylphthalate 27.60 149 909329 11.48 ug/1 # 99 36) Fluoranthene 29.33 202 680237 10.30 ug/1 96 39) Pyrene 30.00 202 705656 14.43 ug/1 # 92 40) Butylbenzylphthalate 32.13 149 328405 13.03 ug/1 97 41) Benzo(a)anthracene 33.64 228 429601 10.57 ug/1 99 42) Bis(2-ethylhexyl)phthalate 33.91 149 459474 13.50 ug/1 95 43) Chrysene 33.77 228 454528 11.40 ug/1 99 45) Di-n-Octylphthalate 35.65 149 568617 12.73 ug/1 # 96 4 6) Benzo(b)fluoranthene 36.75 252 347593m 11.23 ug/1 4 7) Benzo(k)fluoranthene 36.82 252 393170 13.03 ug/1 97 48) Benzo(a)pyrene 37.74 252 252610 8.95 ug/1 # 97 4 9) Indeno(1,2,3 -cd)pyrene 42.06 276 235400 6.91 ug/1 95 5 0) Dibenz(a,h)anthracene 42.14 278 191397 7.26 ug/1 97 51) Benzo(g,h,i)perylene 43.29 276 213330 7.68 ug/1 95

(#) = qualifier out of range (m) = manual integration REF2A.D GCMS0308.M Thu Mar 28 11:13:25 2002 Page 2

NYC-WTC_000011855

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NYC-WTC_000011855Source: NYC Law Department, mirrored locally

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