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GCMS reference standard results, sample AE04948, March 2002

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Reference standard analysis for gas chromatography-mass spectrometry dated March 29, 2002.

NYC-WTC_000058727–000058734

Folder label: “GCMS X 3/7/02 A 3/27/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\MAR26O2\REFA.D Vial: 18 Acq On : 27 Mar 2002 2:33 am Operator: Sample : gc/ms scan 3/7 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 29 11:13 2002 Quant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Mar 29 10:31:28 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 23.21 168 149083 5.59 ug/1 # 82 31) 4-Bromophenyl-phenylether 24.29 248 100824 6.44 ug/1 # 89 32) Hexachlorobenzene 24.73 284 117656 6.47 ug/1 91 33) Phenanthrene 25.70 178 551349 6.47 ug/1 98 34) Anthracene 25.84 178 512808 6.07 ug/1 98 35) Di-n-butylphthalate 27.60 149 698859 6.51 ug/1 99 36) Fluoranthene 29.33 202 532666 5.96 ug/1 # 94 3 9) Pyrene 30.00 202 549162 8.70 ug/1 94 40) Butylbenzylphthalate 32.13 149 224887 6.91 ug/1 # 96 41) Benzo(a)anthracene 33.64 228 319517 6.09 ug/1 99 42) Bis(2-ethylhexyl)phthalate 33.91 149 290748 6.62 ug/1 95 43) Chrysene 33.77 228 352791 6.85 ug/1 99 45) Di-n-Octylphthalate 35.65 149 326714 5.91 ug/1 # 98 46) Benzo(b)fluoranthene 36.75 252 263778 6.89 ug/1 99 47) Benzo(k)fluoranthene 36.82 252 277050m 7.42 ug/1 48) Benzo(a)pyrene 37.74 252 185705 5.32 ug/1 97 49) Indeno(1,2,3-cd)pyrene 42.06 276 176034 4.18 ug/1 99 50) Dibenz(a,h)anthracene 42.13 278 151925 4.65 ug/1 95 51) Benzo(g,h,i)perylene 43.30 276 161254 4.69 ug/1 97

(#) = qualifier out of range (m) = manual integration REFA.D GCMS0308.M Fri Mar 29 11:14:31 2002 Page 2

NYC-WTC_000058730

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NYC-WTC_000058730Source: NYC Law Department, mirrored locally

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