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GCMS analysis results for sample AE01156, March 29 2002

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Gas chromatography-mass spectrometry analysis of sample AE01156 conducted March 29, 2002, showing surrogate standard 2,4-DDD recovery.

NYC-WTC_000059687–000059692

Folder label: “GCMS X 3/13/02 A 3/27/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\MAR2102\REFA2.D Vial: 18 Acq On : 22 Mar 2002 4:03 am Operator: Sample : gc/ms scan 3/13 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 25 9:01 2002 Quant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Mar 08 08:54:27 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 23.23 168 126480 7.75 ug/1 # .81 31) 4-Bromophenyl-phenylether 24.32 248 81600 8.51 ug/1 90 32) Hexachlorobenzene 24.75 284 95779 8.61 ug/1 92 33) Phenanthrene 25.72 178 451632 8.66 ug/1 98 34) Anthracene 25.85 178 423990 8.20 ug/1 98 35) Di-n-butylphthalate 27.62 149 561452 8.55 ug/1 99 36) Fluoranthene 29.35 202 449168 8.21 ug/1 # 93 3 9) Pyrene 30.03 202 463776 10.55 ug/1 # 93 40) Butylbenzylphthalate 32.16 149 209113 9.22 ug/1 98 41) Benzo(a)anthracene 33.66 228 316362 8.65 ug/1 99 42) Bis(2-ethylhexyl)phthalate 33.93 149 277635 9.07 ug/1 95 43) Chrysene 33.79 228 330398 9.21 ug/1 99 45) Di-n-Octylphthalate 35.67 149 323088 7.97 ug/1 # 97 46) Benzo(b)fluoranthene 36.78 252 248736 8.86 ug/1 # 96 47) Benzo(k)fluoranthene 36.84 252 277959 10.15 ug/1 # 96 48) Benzo(a)pyrene 37.78 252 178154 6.96 ug/1 # 97 49) Indeno(1,2,3-cd)pyrene 42.10 276 185318 6.00 ug/1 98 5 0) Dibenz(a,h)anthracene 42.19 278 162609 6.80 ug/1 98 51) Benzo(g,h,i)perylene 43.35 276 163364 6.48 ug/1 97

(#) = qualifier out of range (m) = manual integration REFA2.D GCMS0308.M Mon Mar 25 09:08:43 2002 Page 2

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