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GCMS reference results for sample AE02567, March 2002

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Laboratory report listing quantitative results for volatile organic compounds in sample AE02567 analyzed on March 21, 2002.

NYC-WTC_000038756–000038763

Folder label: “GCMS X 3/4/02 A 3/20/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\MAR1902\REFA2.D Vial: 18 Acq On : 20 Mar 2002 9:44 pm Operator : Sample : gc/ms scan 3/4 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 21 13:49 2002 Quant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Mar 08 08:54:27 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 23.24 168 164563 7.39 ug/1 # 81 31) 4-Bromophenyl-phenylether 24.31 248 109051 8.33 ug/1 93 32) Hexachlorobenzene 24.75 284 115490 7.60 ug/1 # 88 33) Phenanthrene 25.73 178 621887 8.73 ug/1 99 34) Anthracene 25.86 178 592914 8.40 ug/1 98 35) Di-n-butylphthalate 27.63 149 805006 8.98 ug/1 99 36) Fluoranthene 29.35 202 638733 8.55 ug/1 95 39) Pyrene 30.02 202 667095 10.25 ug/1 # 90 40) Butylbenzylphthalate 32.15 149 305982 9.12 ug/1 97 41) Benzo(a)anthracene 33.67 228 478996 8.85 ug/1 98 42) Bis(2-ethylhexyl)phthalate 33.93 149 406523 8.97 ug/1 94 43) Chrysene 33.80 228 504473 9.51 ug/1 99 45) Di-n-Octylphthalate 35.67 149 537096 8.64 ug/1 # 98 46) Benzo(b)fluoranthene 36.78 252 426904 9.91 ug/1 99 47) Benzo(k)fluoranthene 36.84 252 443198m 10.55 ug/1 48) Benzo(a)pyrene 37.77 252 308935 7.87 ug/1 # 96 49) Indeno(1,2,3-cd)pyrene 42.10 276 320329 6.76 ug/1 96 50) Dibenz(a,h)anthracene 42.19 278 286342 7.80 ug/1 96 51) Benzo(g,h,i)perylene 43.35 276 291286 7.53 ug/1 93

(#) = qualifier out of range (m) = manual integration REFA2.D GCMS0308.M Thu Mar 21 13:49:54 2002 Page 2

NYC-WTC_000038759

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NYC-WTC_000038759Source: NYC Law Department, mirrored locally

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