GCMS reference results for sample AE02567, March 2002

NYC 9/11 Public Portal Document Quantitation Keporc (Q1 Reviewed)

Data File : C:\HPCHEM\l\DATA\MAR1902\REFA2.D Vial: 18 E Acq On : 20 Mar 2002 9:44 pm Operator: Sample : gc/ms scan 3/4 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 21 13:49 2002 Quant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Mar 08 08:54:27 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.27 152 509716 20.00 ug/1 -0.08 10) Naphthalene-d8 15.90 136 1986148 20.00 ug/1 -0.09 17) Acenaphthene-diO 21.22 164 1071013 20.00 ug/1 -0.09 29) Phenanthrene-diO 25.66 188 1648691 20.00 ug/1 -0.10 38) Chrysene-dl2 33.72 240 1133211 20.00 ug/1 -0.12 44) Perylene-dl2 37.97 264 705547 20.00 ug/1 -0.15

System Monitoring Compounds 37) 2,4-DDD 30.73 235 90445 7.55 ug/mL 0.23 Spiked Amount 5.000 Recovery = 151.00%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.90 74 82850 4.79 ug/1 # 69 3) bis(2-Chloroethyl)ether 11.65 93 202040 7.26 ug/1 93 4) 1,3-Dichlorobenzene 12.17 146 115436 4.01 ug/1 100 5) 1,4-Dichlorobenzene 12.31 146 128102 4.44 ug/1 99 6) 1,2-Dichlorobenzene 12.83 146 135062 5.02 ug/1 97 7) 2,2‘-oxybis(1-Chloropropan 13.14 45 281187 7.18 ug/1 99 8) N-Nitroso-di-n-propylamine 13.53 70 141420 7.81 ug/1 # 86 9) Hexachloroethane 13.67 117 24782 2.30 ug/1 95 11) Nitrobenzene 13.95 77 188768 6.95 ug/1 90 12) Isophorone 14.59 82 411187 7.99 ug/1 99 13) bis(2-Chloroethoxy)methane 15.28 93 254662 7.56 ug/1 95 14) 1,2,4-Trichlorobenzene 15.79 180 125533 5.38 ug/1 96 15) Naphthalene 15.96 128 527620 7.19 ug/1 98 16) Hexachlorobutadiene 16.50 225 16785 1.44 ug/1 97 18) Hexachlorocyclopentadiene 18.70 237 10054 1.39 ug/1 99 19) 2-Chloronaphthalene 19.47 162 334849 7.28 ug/1 97 20) Dimethylphthalate 20.56 163 478935 8.89 ug/1 98 21) 2,6-Dinitrotoluene 20.77 165 101100 7.73 ug/1 # 85 22) Acenaphthylene 20.74 152 547347 8.33 ug/1 100 23) Acenaphthene 21.30 153 372381 8.10 ug/1 99 24) 2,4-Dinitrotoluene 21.94 165 131273 7.50 ug/1 # 76 25) Diethylphthalate 22.69 149 475525 9.09 ug/1 96 26) 4-Chlorophenyl-phenylether 22.84 204 198745 8.87 ug/1 93 27) Fluorene 22.83 166 430225 8.85 ug/1 98 28) Azobenzen/ 1,2-Diphenylhyd 23.31 77 413221 7.37 ug/L # 85

(#) = qualifier out of range (m) = manual integration REFA2.D GCMS0308.M Thu Mar 21 13:49:50 2002 Page 1

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