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GCMS reference standard analysis, April 2002

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Quantitative results for reference standards analyzed by GCMS on April 3, 2002, to validate analytical accuracy.

NYC-WTC_000058911–000058918

Folder label: “GCMS X 3/8/02 A 3/30/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\MAR3002\REFAl.D Vial: 27 Acq On : 30 Mar 2002 6:45 pm Operator: Sample : gc/ms scan 3/8 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 30 19:33 2002 • Quant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Mar 29 10:31:28 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 23.22 168 148754 7.62 ug/1 # 80 31) 4-Bromophenyl-phenylether 24.29 248 111889 9.76 ug/1 91 32) Hexachlorobenzene 24.73 284 133712 10.04 ug/1 # 89 33) Phenanthrene 25.70 178 595007 9.54 ug/1 98 34) Anthracene 25.83 178 544050 8.79 ug/1 99 35) Di-n-butylphthalate 27.60 149 750304 9.56 ug/1 99 36) Fluoranthene 29.33 202 576024 8.80 ug/1 96 3 9) Pyrene 30.00 202 591068 12.98 ug/1 # 91 40) Butylbenzylphthalate 32.13 149 242423 10.32 ug/1 95 41) Benzo(a)anthracene 33.64 228 347639 9.18 ug/1 99 42) Bis(2-ethylhexyl)phthalate 33.91 149 294607 9.29 ug/1 # 94 43) Chrysene 33.77 228 375131 10.10 ug/1 99 45) Di-n-Octylphthalate 35.65 149 338298 8.50 ug/1 # 97 46) Benzo(b)fluoranthene 36.75 252 267522 9.70 ug/1 # 97 47) Benzo(k)fluoranthene 36.81 252 309455 11.51 ug/1 # 96 48) Benzo(a)pyrene 37.74 252 178230 7.09 ug/1 # 95 49) Indeno(1,2,3-cd)pyrene 42.05 276 186798 6.16 ug/1 # 95 5 0) Dibenz(a,h)anthracene 42.14 278 161369 6.87 ug/1 98 51) Benzo(g,h,i)perylene 43.29 276 166868 6.74 ug/1 96

(#) = qualifier out of range (m) = manual integration REFAl.D GCMS0308.M Tue Apr 02 15:13:06 2002 Page 2

NYC-WTC_000058914

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NYC-WTC_000058914Source: NYC Law Department, mirrored locally

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